Technology Process of C22H29NO4S
There total 7 articles about C22H29NO4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
borane-THF;
In
tetrahydrofuran;
at 0 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/ol2010598
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium tris[(3-ethyl-3-pentyl)oxy]aluminohydride / tetrahydrofuran / 3 h / -78 - 20 °C / Inert atmosphere
2: borane-THF / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
With
borane-THF; lithium tris[(3-ethyl-3-pentyl)oxy]aluminohydride;
In
tetrahydrofuran;
DOI:10.1021/ol2010598
- Guidance literature:
-
Multi-step reaction with 6 steps
1: hydrogenchloride / methanol; water / 12 h / 20 °C / Inert atmosphere
2: triethylamine / tetrahydrofuran / 5 h / 0 °C / Inert atmosphere
3: sodium hydride / tetrahydrofuran / 20 °C / Inert atmosphere
4: N-chloro-succinimide; silver nitrate / water; acetonitrile / 0.08 h / 0 °C / Inert atmosphere
5: lithium tris[(3-ethyl-3-pentyl)oxy]aluminohydride / tetrahydrofuran / 3 h / -78 - 20 °C / Inert atmosphere
6: borane-THF / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
With
hydrogenchloride; N-chloro-succinimide; borane-THF; lithium tris[(3-ethyl-3-pentyl)oxy]aluminohydride; sodium hydride; silver nitrate; triethylamine;
In
tetrahydrofuran; methanol; water; acetonitrile;
DOI:10.1021/ol2010598
