C₃₃H₄₆O₈SiS

Base Information

Chemical Name:C₃₃H₄₆O₈SiS
CAS No.:897044-14-3
Molecular Formula:C₃₃H₄₆O₈SSi
Molecular Weight:630.875
Hs Code.:

C<sub>33</sub>H<sub>46</sub>O<sub>8</sub>SiS

Synonyms:C₃₃H₄₆O₈SiS

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Chemical Property of C₃₃H₄₆O₈SiS

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Technology Process of C₃₃H₄₆O₈SiS

There total 2 articles about C₃₃H₄₆O₈SiS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 897044-01-8
C₃₈H₅₈O₈SiS₃

: 897044-14-3
C₃₃H₄₆O₈SiS

Guidance literature:: Multi-step reaction with 3 steps

1.1: mCPBA / CH₂Cl₂

1.2: 94 percent / camphorsulfonic acid / various solvent(s) / 6 h / 20 °C

2.1: 97 percent / trimethylsilyl chloride; water / CH₂Cl₂ / 0 °C

3.1: 76 percent / CH₃SO₂Cl; triethylamine / CH₂Cl₂ / 21 h / -10 - 20 °C

With chloro-trimethyl-silane; water; methanesulfonyl chloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1002/anie.200504033

Reference yield:

: 897044-04-1
C₃₅H₅₂O₁₀SiS

: 897044-14-3
C₃₃H₄₆O₈SiS

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / trimethylsilyl chloride; water / CH₂Cl₂ / 0 °C

2: 76 percent / CH₃SO₂Cl; triethylamine / CH₂Cl₂ / 21 h / -10 - 20 °C

With chloro-trimethyl-silane; water; methanesulfonyl chloride; triethylamine; In dichloromethane;
DOI:10.1002/anie.200504033

Reference yield:

: 897044-14-3
C₃₃H₄₆O₈SiS

: 897044-17-6
C₄₀H₆₄O₉Si₂S

Guidance literature:: Multi-step reaction with 2 steps

1: PhSNa

2: 2,6-lutidine / CH₂Cl₂ / -20 - 20 °C

With 2,6-dimethylpyridine; sodium thiophenolate; In dichloromethane;
DOI:10.1002/anie.200504033