2-[1-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-propyl]-propenal

Base Information

• Chemical Name: 2-[1-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-propyl]-propenal
• CAS No.: 900796-49-8
• Molecular Formula: C₂₀H₃₂O₄Si
• Molecular Weight: 364.557

Synonyms:2-[1-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-propyl]-propenal

Chemical Property of 2-[1-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-propyl]-propenal

Chemical Property:

Purity/Quality:

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Technology Process of 2-[1-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-propyl]-propenal

There total 4 articles about 2-[1-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-propyl]-propenal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(p-methoxybenzyloxy)propanal (128461-65-4) → 2-[1-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-propyl]-propenal (900796-49-8)

Guidance literature:

Multi-step reaction with 4 steps

1: 62 percent / 3-hydroxy-quinuclidine

2: 90 percent / imidazole; DMAP / dimethylformamide / 16 h / 20 °C

3: DIBAL / CH₂Cl₂

4: MnO₂ / CH₂Cl₂ / Heating

With 1H-imidazole; dmap; manganese(IV) oxide; diisobutylaluminium hydride; 3-quinuclidinol; In dichloromethane; N,N-dimethyl-formamide; 1: Baylis-Hillman reaction;

DOI:10.1016/j.tetlet.2006.04.071

Reference yield:

2-[1-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-propyl]-prop-2-en-1-ol → 2-[1-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-propyl]-propenal (900796-49-8)

Guidance literature:

With manganese(IV) oxide; In dichloromethane; Heating;

DOI:10.1016/j.tetlet.2006.04.071

Reference yield:

2-[1-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-propyl]-acrylic acid methyl ester (900796-48-7) → 2-[1-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-propyl]-propenal (900796-49-8)

Guidance literature:

Multi-step reaction with 2 steps

1: DIBAL / CH₂Cl₂

2: MnO₂ / CH₂Cl₂ / Heating

With manganese(IV) oxide; diisobutylaluminium hydride; In dichloromethane;

DOI:10.1016/j.tetlet.2006.04.071

upstream raw materials:

2-[1-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-propyl]-acrylic acid methyl ester

3-(p-methoxybenzyloxy)propanal

2-(1-hydroxy-3-p-methoxybenzyloxypropyl)acrylic acid methyl ester

Downstream raw materials:

4-[1-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-propyl]-penta-2,4-dienoic acid methyl ester

(E)-(2S,3R,7R)-1-((S)-4-Benzyl-5,5-diphenyl-2-thioxo-oxazolidin-3-yl)-7-(tert-butyl-dimethyl-silanyloxy)-3-hydroxy-9-(4-methoxy-benzyloxy)-2-methyl-6-methylene-non-4-en-1-one

(E)-(2S,3R,7S)-1-((S)-4-Benzyl-5,5-diphenyl-2-thioxo-oxazolidin-3-yl)-7-(tert-butyl-dimethyl-silanyloxy)-3-hydroxy-9-(4-methoxy-benzyloxy)-2-methyl-6-methylene-non-4-en-1-one

4-[1-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-propyl]-penta-2,4-dienal

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