3-carbamoyl>acrylate

Base Information

• Chemical Name: 3-carbamoyl>acrylate
• CAS No.: 106909-25-5
• Molecular Formula: C₂₂H₂₅NO₄
• Molecular Weight: 367.445

Synonyms:3-carbamoyl>acrylate

Chemical Property of 3-carbamoyl>acrylate

Chemical Property:

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Technology Process of 3-carbamoyl>acrylate

There total 1 articles about 3-carbamoyl>acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

fumaric acid ethyl ester mono chloride (26367-48-6) + 2-(benzylamino)-α,α-dimethylbenzyl alcohol (106899-21-2) → 3-carbamoyl>acrylate (106909-25-5)

Guidance literature:

With sodium hydrogencarbonate; In dichloromethane; for 1h;

DOI:10.1248/cpb.34.140

Reference yield: 50.0%

3-carbamoyl>acrylate (106909-25-5) → ethyl 1-benzyl=1,2,3,5-tetrahydro-5,5-dimethyl-2-oxo-4,1-benzoxazepine-3-acetate (82669-46-3)

Guidance literature:

With potassium carbonate; In ethanol; for 3h; Ambient temperature;

DOI:10.1248/cpb.34.140

upstream raw materials:

fumaric acid ethyl ester mono chloride

2-(benzylamino)-α,α-dimethylbenzyl alcohol

Downstream raw materials:

ethyl 1-benzyl=1,2,3,5-tetrahydro-5,5-dimethyl-2-oxo-4,1-benzoxazepine-3-acetate

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