(3R,4S,5S)-3-amino-5-(4-methoxy-3-propyl-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride

Base Information

Chemical Name:(3R,4S,5S)-3-amino-5-(4-methoxy-3-propyl-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride
CAS No.:947319-98-4
Molecular Formula:C₁₆H₂₅NO₄S*ClH
Molecular Weight:363.906
Hs Code.:

Synonyms:(3R,4S,5S)-3-amino-5-(4-methoxy-3-propyl-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride

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Chemical Property of (3R,4S,5S)-3-amino-5-(4-methoxy-3-propyl-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride

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Technology Process of (3R,4S,5S)-3-amino-5-(4-methoxy-3-propyl-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride

There total 1 articles about (3R,4S,5S)-3-amino-5-(4-methoxy-3-propyl-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 947319-97-3
(3aR,7S,7aS)-7-[4-methoxy-3-propyl-benzyl]-2,2-dimethyl-5,5-dioxo-hexahydro-1-oxa-5λ6-thia-3-aza-indene-3-carboxylic acid tert-butyl ester

: 947319-98-4
(3R,4S,5S)-3-amino-5-(4-methoxy-3-propyl-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride

Guidance literature:: (3aR,7S,7aS)-7-[4-methoxy-3-propyl-benzyl]-2,2-dimethyl-5,5-dioxo-hexahydro-1-oxa-5λ6-thia-3-aza-indene-3-carboxylic acid tert-butyl ester; With hydrogenchloride; In 1,4-dioxane; at 25 ℃; for 2h;

With hydrogenchloride; methanol; water; at 25 ℃; for 0.5h;

Reference yield:

: 947319-98-4
(3R,4S,5S)-3-amino-5-(4-methoxy-3-propyl-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride

: 34246-57-6
3-isopropylbenzaldehyde

: (3R,4S,5S)-3-(3-isopropyl-benzylamino)-5-(4-methoxy-3-propyl-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol

Guidance literature:: (3R,4S,5S)-3-amino-5-(4-methoxy-3-propyl-benzyl)-1,1-dioxo-hexahydro-1λ6-thiopyran-4-ol hydrochloride; 3-isopropylbenzaldehyde; With sodium acetate; In methanol; dichloromethane; at 25 ℃; for 0.5h;

With sodium cyanoborohydride; In methanol; dichloromethane; for 1h;

With hydrogenchloride; water; potassium carbonate; more than 3 stages;