C₄₁H₅₃BrO₆Si

Base Information

Chemical Name:C₄₁H₅₃BrO₆Si
CAS No.:1315567-66-8
Molecular Formula:C₄₁H₅₃BrO₆Si
Molecular Weight:749.858
Hs Code.:

C<sub>41</sub>H<sub>53</sub>BrO<sub>6</sub>Si

Synonyms:C₄₁H₅₃BrO₆Si

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Chemical Property of C₄₁H₅₃BrO₆Si

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Technology Process of C₄₁H₅₃BrO₆Si

There total 10 articles about C₄₁H₅₃BrO₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1315567-83-9
C₃₃H₄₇BrO₆Si

: 536-74-3
phenylacetylene

: 1315567-66-8
C₄₁H₅₃BrO₆Si

Guidance literature:: With methyllithium lithium bromide; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1038/nchem.1074

Reference yield:

: 1315567-82-8
C₃₉H₆₂O₇Si₂

: 1315567-66-8
C₄₁H₅₃BrO₆Si

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; dibromo sulfoxide / diethyl ether / -40 °C

2: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0 °C

3: methyllithium lithium bromide / tetrahydrofuran / -78 - 20 °C

With pyridine; dibromo sulfoxide; methyllithium lithium bromide; tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; diethyl ether;
DOI:10.1038/nchem.1074

Reference yield:

: C₁₈H₂₃BrO₃

: 1315567-66-8
C₄₁H₅₃BrO₆Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: isopropyl alcohol / 80 °C

2.1: 122 °C / neat (no solvent)

2.2: 20 °C

3.1: 1,2-dichloro-benzene / 250 °C / Microwave irradiation

4.1: iodine; magnesium / diethyl ether / 0 °C

5.1: pyridine; dibromo sulfoxide / diethyl ether / -40 °C

6.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0 °C

7.1: methyllithium lithium bromide / tetrahydrofuran / -78 - 20 °C

With pyridine; dibromo sulfoxide; methyllithium lithium bromide; tetrabutyl ammonium fluoride; iodine; magnesium; acetic acid; In tetrahydrofuran; diethyl ether; 1,2-dichloro-benzene; isopropyl alcohol; 2.1: Claisen rearrangement;
DOI:10.1038/nchem.1074