N,N,N',N'-tetrakis(2-fluoro-2,2-dinitroethyl)oxamide

Base Information

Chemical Name:N,N,N',N'-tetrakis(2-fluoro-2,2-dinitroethyl)oxamide
CAS No.:80036-97-1
Molecular Formula:C₁₀H₈F₄N₁₀O₁₈
Molecular Weight:632.223
Hs Code.:
Mol file:80036-97-1.mol

Synonyms:Ethanediamide,tetrakis(2-fluoro-2,2-dinitroethyl)- (9CI)

Suppliers and Price of N,N,N',N'-tetrakis(2-fluoro-2,2-dinitroethyl)oxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of N,N,N',N'-tetrakis(2-fluoro-2,2-dinitroethyl)oxamide

Chemical Property:

Boiling Point:629.8±65.0 °C(Predicted)
PKA:-2.44±0.70(Predicted)
Flash Point:334.7oC
PSA：407.18000
Density:1.935±0.06 g/cm3(Predicted)
LogP:1.53600

Purity/Quality:: 99%+ ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N,N,N',N'-tetrakis(2-fluoro-2,2-dinitroethyl)oxamide

There total 6 articles about N,N,N',N'-tetrakis(2-fluoro-2,2-dinitroethyl)oxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 80036-96-0
1,2'-azobis

: 80036-97-1
N,N,N',N'-tetrakis(2-fluoro-2,2-dinitroethyl)oxamide

Guidance literature:: at 150 - 160 ℃; for 0.333333h;
DOI:10.1021/je00027a031

Reference yield:

: 54373-81-8
N,N-bis(2-fluoro-2,2-dinitroethyl)-carbamyl chloride

: 80036-97-1
N,N,N',N'-tetrakis(2-fluoro-2,2-dinitroethyl)oxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / pyridine / diethyl ether

2: 96 percent / 70percent nitric acid / 5 h / Ambient temperature

3: 36 percent / 0.33 h / 150 - 160 °C

With pyridine; nitric acid; In diethyl ether;
DOI:10.1021/je00027a031

Reference yield:

: 79059-77-1
S-ethyl N,N-bis-(2-fluoro-2,2-dinitroethyl)thiocarbamate

: 80036-97-1
N,N,N',N'-tetrakis(2-fluoro-2,2-dinitroethyl)oxamide

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / SO₂Cl₂ / 1,2-dichloro-ethane / 8 h / Heating

2: 83 percent / pyridine / diethyl ether

3: 96 percent / 70percent nitric acid / 5 h / Ambient temperature

4: 36 percent / 0.33 h / 150 - 160 °C

With pyridine; sulfuryl dichloride; nitric acid; In diethyl ether; 1,2-dichloro-ethane;
DOI:10.1021/je00027a031