Technology Process of C75H121N3O8S
There total 4 articles about C75H121N3O8S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran;
at 20 ℃;
DOI:10.1016/j.bmcl.2011.06.004
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium aluminium tetrahydride / tetrahydrofuran
2: dmap; diisopropyl-carbodiimide / dichloromethane / 20 °C
3: piperidine; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 20 °C
4: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C
With
piperidine; dmap; lithium aluminium tetrahydride; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2011.06.004
- Guidance literature:
-
Multi-step reaction with 5 steps
1: desipramine; potassium carbonate
2: lithium aluminium tetrahydride / tetrahydrofuran
3: dmap; diisopropyl-carbodiimide / dichloromethane / 20 °C
4: piperidine; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 20 °C
5: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C
With
piperidine; dmap; lithium aluminium tetrahydride; desipramine; potassium carbonate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2011.06.004