3-chloro-N-(2-(3-(cyclopropylmethoxy)phenyl)propan-2-yl)propane-1-sulfonamide

Base Information

Chemical Name:3-chloro-N-(2-(3-(cyclopropylmethoxy)phenyl)propan-2-yl)propane-1-sulfonamide
CAS No.:1369704-41-5
Molecular Formula:C₁₆H₂₄ClNO₃S
Molecular Weight:345.89
Hs Code.:

Synonyms:3-chloro-N-(2-(3-(cyclopropylmethoxy)phenyl)propan-2-yl)propane-1-sulfonamide

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Chemical Property of 3-chloro-N-(2-(3-(cyclopropylmethoxy)phenyl)propan-2-yl)propane-1-sulfonamide

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Technology Process of 3-chloro-N-(2-(3-(cyclopropylmethoxy)phenyl)propan-2-yl)propane-1-sulfonamide

There total 4 articles about 3-chloro-N-(2-(3-(cyclopropylmethoxy)phenyl)propan-2-yl)propane-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1633-82-5
3-chloro-n-propanesulfonyl chloride

: 1198223-53-8
2-(3-(cyclopropylmethoxy)phenyl)propan-2-amine

: 1369704-41-5
3-chloro-N-(2-(3-(cyclopropylmethoxy)phenyl)propan-2-yl)propane-1-sulfonamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jm201628y

Reference yield:

: 1-(2-azidopropan-2-yl)-3-(cyclopropylmethoxy)benzene

: 1369704-41-5
3-chloro-N-(2-(3-(cyclopropylmethoxy)phenyl)propan-2-yl)propane-1-sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 - 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm201628y

Reference yield:

: 1150617-70-1
methyl 3-(cyclopropylmethoxy)benzoate

: 1369704-41-5
3-chloro-N-(2-(3-(cyclopropylmethoxy)phenyl)propan-2-yl)propane-1-sulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran; diethyl ether / 4 h / 0 - 20 °C / Inert atmosphere

2: sodium azide; trifluoroacetic acid / chloroform / 1 h / 0 - 20 °C / Inert atmosphere

3: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 - 20 °C / Inert atmosphere

4: triethylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium azide; triethylamine; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; chloroform;
DOI:10.1021/jm201628y