(E)-4-benzoyloxy-3-methyl-2-butenyl-1,1-difluoro phosphonic acid

Base Information

Chemical Name:(E)-4-benzoyloxy-3-methyl-2-butenyl-1,1-difluoro phosphonic acid
CAS No.:1113039-88-5
Molecular Formula:C₁₂H₁₃F₂O₅P
Molecular Weight:306.203
Hs Code.:

Synonyms:(E)-4-benzoyloxy-3-methyl-2-butenyl-1,1-difluoro phosphonic acid

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Chemical Property of (E)-4-benzoyloxy-3-methyl-2-butenyl-1,1-difluoro phosphonic acid

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Technology Process of (E)-4-benzoyloxy-3-methyl-2-butenyl-1,1-difluoro phosphonic acid

There total 1 articles about (E)-4-benzoyloxy-3-methyl-2-butenyl-1,1-difluoro phosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1113039-87-4
(E)-4-(diethoxyphosphoryl)-4,4-difluoro-2-methylbut-2-enyl benzoate

: 1113039-88-5
(E)-4-benzoyloxy-3-methyl-2-butenyl-1,1-difluoro phosphonic acid

Guidance literature:: (E)-4-(diethoxyphosphoryl)-4,4-difluoro-2-methylbut-2-enyl benzoate; With trimethylsilyl bromide; In acetonitrile; at 20 ℃; for 12h;

With methanol; at 20 ℃; for 0.5h;
DOI:10.1002/anie.200803452

Reference yield: 64.0%

: 1113039-88-5
(E)-4-benzoyloxy-3-methyl-2-butenyl-1,1-difluoro phosphonic acid

: triammonium (E)-4-benzoyloxy-3-methyl-2-butenyl-1,1-difluoro pyrophosphonate

Guidance literature:: (E)-4-benzoyloxy-3-methyl-2-butenyl-1,1-difluoro phosphonic acid; With tributyl-amine; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; at 20 ℃; for 3h; Further stages;
DOI:10.1002/anie.200803452