tert-butyl N-[2-(1,1-dioxo-4-phenyl-λ⁶-thian-4-yl)ethyl]carbamate

Base Information

Chemical Name:tert-butyl N-[2-(1,1-dioxo-4-phenyl-λ⁶-thian-4-yl)ethyl]carbamate
CAS No.:1581258-40-3
Molecular Formula:C₁₈H₂₇NO₄S
Molecular Weight:353.483
Hs Code.:

tert-butyl N-[2-(1,1-dioxo-4-phenyl-λ<sup>6</sup>-thian-4-yl)ethyl]carbamate

Synonyms:tert-butyl N-[2-(1,1-dioxo-4-phenyl-λ⁶-thian-4-yl)ethyl]carbamate

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Chemical Property of tert-butyl N-[2-(1,1-dioxo-4-phenyl-λ⁶-thian-4-yl)ethyl]carbamate

Chemical Property:

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Technology Process of tert-butyl N-[2-(1,1-dioxo-4-phenyl-λ⁶-thian-4-yl)ethyl]carbamate

There total 6 articles about tert-butyl N-[2-(1,1-dioxo-4-phenyl-λ⁶-thian-4-yl)ethyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1581258-39-0
tert-butyl 2-(4-phenyltetrahydro-2H-thiopyran-4-yl)ethylcarbamate

: 1581258-40-3
tert-butyl N-[2-(1,1-dioxo-4-phenyl-λ⁶-thian-4-yl)ethyl]carbamate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 64h; Cooling;

Reference yield:

: 10292-84-9
ethyl 2-cyano-2-(2H-thiopyran-4(3H,5H,6H)-ylidene)acetate

: 1581258-40-3
tert-butyl N-[2-(1,1-dioxo-4-phenyl-λ⁶-thian-4-yl)ethyl]carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: diethyl ether / 1 h / Reflux

2: potassium hydroxide / ethylene glycol / 2 h / 190 °C

3: sodium tetrahydroborate; cobalt(II) chloride; methanol / 0.5 h / 0 - 20 °C

4: N-ethyl-N,N-diisopropylamine / methanol; dichloromethane / 20 °C

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 64 h / 20 °C / Cooling

With methanol; sodium tetrahydroborate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; cobalt(II) chloride; potassium hydroxide; In methanol; diethyl ether; dichloromethane; ethylene glycol;

Reference yield:

: 1072-72-6
Tetrahydrothiopyran-4-one

: 1581258-40-3
tert-butyl N-[2-(1,1-dioxo-4-phenyl-λ⁶-thian-4-yl)ethyl]carbamate

Guidance literature:: Multi-step reaction with 6 steps

1: ammonium acetate / toluene / 48 h / 150 °C

2: diethyl ether / 1 h / Reflux

3: potassium hydroxide / ethylene glycol / 2 h / 190 °C

4: sodium tetrahydroborate; cobalt(II) chloride; methanol / 0.5 h / 0 - 20 °C

5: N-ethyl-N,N-diisopropylamine / methanol; dichloromethane / 20 °C

6: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 64 h / 20 °C / Cooling

With methanol; sodium tetrahydroborate; ammonium acetate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; cobalt(II) chloride; potassium hydroxide; In methanol; diethyl ether; dichloromethane; ethylene glycol; toluene;