2,2-bis-(3,5-di-tert-butyl-4-hydroxybenzyl)-malonic acid di-[4-(1,1,3,3-tetramethylbutyl)-phenyl]-ester

Base Information

• Chemical Name: 2,2-bis-(3,5-di-tert-butyl-4-hydroxybenzyl)-malonic acid di-[4-(1,1,3,3-tetramethylbutyl)-phenyl]-ester
• CAS No.: 39266-77-8
• Molecular Formula: C₆₁H₈₈O₆
• Molecular Weight: 917.366

Synonyms:2,2-bis-(3,5-di-tert-butyl-4-hydroxybenzyl)-malonic acid di-[4-(1,1,3,3-tetramethylbutyl)-phenyl]-ester

Chemical Property of 2,2-bis-(3,5-di-tert-butyl-4-hydroxybenzyl)-malonic acid di-[4-(1,1,3,3-tetramethylbutyl)-phenyl]-ester

Chemical Property:

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Technology Process of 2,2-bis-(3,5-di-tert-butyl-4-hydroxybenzyl)-malonic acid di-[4-(1,1,3,3-tetramethylbutyl)-phenyl]-ester

There total 2 articles about 2,2-bis-(3,5-di-tert-butyl-4-hydroxybenzyl)-malonic acid di-[4-(1,1,3,3-tetramethylbutyl)-phenyl]-ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-octylphenol (140-66-9) → 2,2-bis-(3,5-di-tert-butyl-4-hydroxybenzyl)-malonic acid di-[4-(1,1,3,3-tetramethylbutyl)-phenyl]-ester (39266-77-8)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂

2: (i) NaOMe, MeOH, toluene, (ii) /BRN= 2052292/, PE

With thionyl chloride;

DOI:10.1002/hlca.19760590218

Reference yield:

3,5-di-tert-butyl-4-hydroxy benzyl chloride (955-01-1) + Malonic acid bis-[4-(1,1,3,3-tetramethyl-butyl)-phenyl] ester (60309-97-9) → 2,2-bis-(3,5-di-tert-butyl-4-hydroxybenzyl)-malonic acid di-[4-(1,1,3,3-tetramethylbutyl)-phenyl]-ester (39266-77-8)

Guidance literature:

Multistep reaction; (i) NaOMe, MeOH, toluene, (ii) /BRN= 2052292/, PE;

DOI:10.1002/hlca.19760590218

upstream raw materials:

3,5-di-tert-butyl-4-hydroxy benzyl chloride

Malonic acid bis-[4-(1,1,3,3-tetramethyl-butyl)-phenyl] ester

tert-octylphenol

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