C₄₆H₇₃N₅O₁₁S

Base Information

Chemical Name:C₄₆H₇₃N₅O₁₁S
CAS No.:1239985-38-6
Molecular Formula:C₄₆H₇₃N₅O₁₁S
Molecular Weight:904.179
Hs Code.:

C<sub>46</sub>H<sub>73</sub>N<sub>5</sub>O<sub>11</sub>S

Synonyms:C₄₆H₇₃N₅O₁₁S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₆H₇₃N₅O₁₁S

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Technology Process of C₄₆H₇₃N₅O₁₁S

There total 14 articles about C₄₆H₇₃N₅O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1352449-79-6
C₆₁H₈₃N₅O₁₃S

: 1239985-38-6
C₄₆H₇₃N₅O₁₁S

Guidance literature:: With diethylamine; In acetonitrile;
DOI:10.1016/j.tet.2011.10.094

Reference yield:

: 1204215-22-4
C₈H₁₄Cl₃NO₂*ClH

: 1239985-38-6
C₄₆H₇₃N₅O₁₁S

Guidance literature:: Multi-step reaction with 12 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane; N,N-dimethyl-formamide / 6 h / 20 °C

2: hydrogenchloride / 1,4-dioxane / 1 h / 10 - 15 °C

3: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 12 h / 20 °C

4: hydrogenchloride / 1,4-dioxane / 1 h / 0 °C

5: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 22 h

6: hydrogenchloride / 1,4-dioxane

7: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane; N,N-dimethyl-formamide / 25 h

8: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h

9: pyridine hydrogenfluoride

10: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h / 0 - 20 °C

11: water; silver nitrate; zinc / tetrahydrofuran

12: diethylamine / acetonitrile

With hydrogenchloride; dmap; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; pyridine hydrogenfluoride; silver nitrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; triethylamine; N-ethyl-N,N-diisopropylamine; zinc; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2011.10.094

Reference yield:

: 1352449-74-1
C₄₅H₆₉Cl₃N₄O₁₀S

: 1239985-38-6
C₄₆H₇₃N₅O₁₁S

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h / 0 - 20 °C

2: water; silver nitrate; zinc / tetrahydrofuran

3: diethylamine / acetonitrile

With dmap; water; silver nitrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; zinc; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2011.10.094