(R)-4-methyl-2-(2-methylallyl)-1-phenyl-1,2,3,6-tetrahydropyridine

Base Information

• Chemical Name: (R)-4-methyl-2-(2-methylallyl)-1-phenyl-1,2,3,6-tetrahydropyridine
• CAS No.: 1114570-92-1
• Molecular Formula: C₁₆H₂₁N
• Molecular Weight: 227.349
• Mol file: 1114570-92-1.mol

Synonyms:(R)-4-methyl-2-(2-methylallyl)-1-phenyl-1,2,3,6-tetrahydropyridine

Chemical Property of (R)-4-methyl-2-(2-methylallyl)-1-phenyl-1,2,3,6-tetrahydropyridine

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (R)-4-methyl-2-(2-methylallyl)-1-phenyl-1,2,3,6-tetrahydropyridine

There total 2 articles about (R)-4-methyl-2-(2-methylallyl)-1-phenyl-1,2,3,6-tetrahydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Z)-N-(4-(allyloxy)but-2-enyl)-N-(2,6-dimethylhepta-1,6-dien-4-yl)aniline (1196496-71-5) → (R)-4-methyl-2-(2-methylallyl)-1-phenyl-1,2,3,6-tetrahydropyridine (1114570-92-1) + (S)-4-methyl-2-(2-methylallyl)-1-phenyl-1,2,3,6-tetrahydropyridine

Guidance literature:

With C₅H₁₂*C₅₄H₇₀Br₂MoN₂O₂Si; In benzene; at 22 ℃; for 1h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;

DOI:10.1021/ja907805f

Reference yield:

allyl[3-methyl-1-(2-methylallyl)but-3-enyl]phenylamine → (R)-4-methyl-2-(2-methylallyl)-1-phenyl-1,2,3,6-tetrahydropyridine (1114570-92-1) + (S)-4-methyl-2-(2-methylallyl)-1-phenyl-1,2,3,6-tetrahydropyridine

Guidance literature:

C₅₂H₅₈Br₂MoN₂O₂Si; In benzene; at 22 ℃; for 12h; Product distribution / selectivity;

upstream raw materials:

(Z)-N-(4-(allyloxy)but-2-enyl)-N-(2,6-dimethylhepta-1,6-dien-4-yl)aniline