4-(5-amino-5-iminopentylcarbamoyl)-2-(3-chlorobenzo[b]thiophene-2-carboxamido)benzoic acid

Base Information

Chemical Name:4-(5-amino-5-iminopentylcarbamoyl)-2-(3-chlorobenzo[b]thiophene-2-carboxamido)benzoic acid
CAS No.:1374778-29-6
Molecular Formula:C₂₂H₂₁ClN₄O₄S
Molecular Weight:472.952
Hs Code.:

Synonyms:4-(5-amino-5-iminopentylcarbamoyl)-2-(3-chlorobenzo[b]thiophene-2-carboxamido)benzoic acid

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Chemical Property of 4-(5-amino-5-iminopentylcarbamoyl)-2-(3-chlorobenzo[b]thiophene-2-carboxamido)benzoic acid

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Technology Process of 4-(5-amino-5-iminopentylcarbamoyl)-2-(3-chlorobenzo[b]thiophene-2-carboxamido)benzoic acid

There total 5 articles about 4-(5-amino-5-iminopentylcarbamoyl)-2-(3-chlorobenzo[b]thiophene-2-carboxamido)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 21815-91-8
3-chlorobenzo[b]thiophen-2-carbonyl chloride

: 1374779-64-2
C₂₂H₁₈ClN₃O₄S

: 1374778-29-6
4-(5-amino-5-iminopentylcarbamoyl)-2-(3-chlorobenzo[b]thiophene-2-carboxamido)benzoic acid

Guidance literature:: 3-chlorobenzo[b]thiophen-2-carbonyl chloride; C₂₂H₁₈ClN₃O₄S; With hydrogenchloride; In ethanol; at 0 - 5 ℃; for 3h;

With ammonia; In ethanol; at 0 - 20 ℃; for 8h;

Reference yield:

: 1374779-62-0
methyl 2-amino-5-carboxybenzoate

: 1374778-29-6
4-(5-amino-5-iminopentylcarbamoyl)-2-(3-chlorobenzo[b]thiophene-2-carboxamido)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 5 h / Reflux

2.1: sodium hydroxide / tetrahydrofuran; ethanol / 3 h / 20 °C

3.1: hydrogenchloride / ethanol / 3 h / 0 - 5 °C

3.2: 8 h / 0 - 20 °C

With hydrogenchloride; sodium hydroxide; In tetrahydrofuran; ethanol;

Reference yield:

: 1374779-63-1
C₂₃H₂₀ClN₃O₄S

: 1374778-29-6
4-(5-amino-5-iminopentylcarbamoyl)-2-(3-chlorobenzo[b]thiophene-2-carboxamido)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / tetrahydrofuran; ethanol / 3 h / 20 °C

2.1: hydrogenchloride / ethanol / 3 h / 0 - 5 °C

2.2: 8 h / 0 - 20 °C

With hydrogenchloride; sodium hydroxide; In tetrahydrofuran; ethanol;