N,N'-di(2-decyltetradecyl)-[2,3-d:6,7-d']-bi[2-(1,3-dithiacyclopenten-2-ylidene)-2-phenyl acetonitrile]naphthalene-1,4,5,8-tetracarboxylic acid diimide

Base Information

Chemical Name:N,N'-di(2-decyltetradecyl)-[2,3-d:6,7-d']-bi[2-(1,3-dithiacyclopenten-2-ylidene)-2-phenyl acetonitrile]naphthalene-1,4,5,8-tetracarboxylic acid diimide
CAS No.:1257635-56-5
Molecular Formula:C₈₀H₁₀₈N₄O₄S₄
Molecular Weight:1318.03
Hs Code.:

N,N'-di(2-decyltetradecyl)-[2,3-d:6,7-d']-bi[2-(1,3-dithiacyclopenten-2-ylidene)-2-phenyl acetonitrile]naphthalene-1,4,5,8-tetracarboxylic acid diimide

Synonyms:N,N'-di(2-decyltetradecyl)-[2,3-d:6,7-d']-bi[2-(1,3-dithiacyclopenten-2-ylidene)-2-phenyl acetonitrile]naphthalene-1,4,5,8-tetracarboxylic acid diimide

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Chemical Property of N,N'-di(2-decyltetradecyl)-[2,3-d:6,7-d']-bi[2-(1,3-dithiacyclopenten-2-ylidene)-2-phenyl acetonitrile]naphthalene-1,4,5,8-tetracarboxylic acid diimide

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Technology Process of N,N'-di(2-decyltetradecyl)-[2,3-d:6,7-d']-bi[2-(1,3-dithiacyclopenten-2-ylidene)-2-phenyl acetonitrile]naphthalene-1,4,5,8-tetracarboxylic acid diimide

There total 3 articles about N,N'-di(2-decyltetradecyl)-[2,3-d:6,7-d']-bi[2-(1,3-dithiacyclopenten-2-ylidene)-2-phenyl acetonitrile]naphthalene-1,4,5,8-tetracarboxylic acid diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: N,N'-di(2-butyloctyl)-[2,3-d:6,7-d']-bi[α,β-dicyanothiophene]naphthalene-1,4,5,8-tetracarboxylic acid diimide

: 140-29-4
phenylacetonitrile

: 1257635-56-5
N,N'-di(2-decyltetradecyl)-[2,3-d:6,7-d']-bi[2-(1,3-dithiacyclopenten-2-ylidene)-2-phenyl acetonitrile]naphthalene-1,4,5,8-tetracarboxylic acid diimide

Guidance literature:: carbon disulfide; phenylacetonitrile; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 2.5h; Inert atmosphere;

N,N'-di(2-butyloctyl)-[2,3-d:6,7-d']-bi[α,β-dicyanothiophene]naphthalene-1,4,5,8-tetracarboxylic acid diimide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.5h;

Reference yield:

: 299962-88-2
2,3,6,7-tetrabromonaphthalene-1,4,5,8-tetracarboxylic dianhydride

: 1257635-56-5
N,N'-di(2-decyltetradecyl)-[2,3-d:6,7-d']-bi[2-(1,3-dithiacyclopenten-2-ylidene)-2-phenyl acetonitrile]-naphthalene-1,4,5,8-tetracarboxylic acid diimide

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / 120 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 - 5 °C / Inert atmosphere

2.2: 2 h / 20 °C

2.3: 0.5 h / 20 °C

With sodium hydride; In acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 62281-07-6
2-decyl-1-tetradecylamine

: 1257635-56-5
N,N'-di(2-decyltetradecyl)-[2,3-d:6,7-d']-bi[2-(1,3-dithiacyclopenten-2-ylidene)-2-phenyl acetonitrile]-naphthalene-1,4,5,8-tetracarboxylic acid diimide

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / 120 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 - 5 °C / Inert atmosphere

2.2: 2 h / 20 °C

2.3: 0.5 h / 20 °C

With sodium hydride; In acetic acid; N,N-dimethyl-formamide;