bis-(4-[{N-(2-acetic acid)-N-methyl}sulfonamido]phenyl)disulfide

Base Information

Chemical Name:bis-(4-[{N-(2-acetic acid)-N-methyl}sulfonamido]phenyl)disulfide
CAS No.:287407-10-7
Molecular Formula:C₂₆H₃₆N₂O₈S₄
Molecular Weight:632.844
Hs Code.:

Synonyms:bis-(4-[{N-(2-acetic acid)-N-methyl}sulfonamido]phenyl)disulfide

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Chemical Property of bis-(4-[{N-(2-acetic acid)-N-methyl}sulfonamido]phenyl)disulfide

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Technology Process of bis-(4-[{N-(2-acetic acid)-N-methyl}sulfonamido]phenyl)disulfide

There total 1 articles about bis-(4-[{N-(2-acetic acid)-N-methyl}sulfonamido]phenyl)disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 287407-07-2
tert-butyl 2-(4-fluoro-N-methylphenylsulfonamido)acetate

: 287407-10-7
bis-(4-[{N-(2-acetic acid)-N-methyl}sulfonamido]phenyl)disulfide

Guidance literature:: tert-butyl 2-(4-fluoro-N-methylphenylsulfonamido)acetate; With potassium ethyl xanthogenate; In dimethyl sulfoxide; at 100 ℃; for 24h;

With bromine; In dichloromethane; at 0 - 20 ℃;

Reference yield: 80.0%

: 287407-10-7
bis-(4-[{N-(2-acetic acid)-N-methyl}sulfonamido]phenyl)disulfide

: 3355-28-0
1-Bromo-2-butyne

: 287407-11-8
2-[(4-but-2-ynylthiophenylsulfonyl)methylamino]acetic acid tert-butyl ester

Guidance literature:: bis-(4-[{N-(2-acetic acid)-N-methyl}sulfonamido]phenyl)disulfide; With hydrogenchloride; triphenylphosphine; In 1,4-dioxane; water; at 20 ℃; for 3h;

With sodium hydride; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 0.5h;

1-Bromo-2-butyne; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 0.5h;