1-(4'-methoxy-2,3,5,6-tetra(1H-pyrazol-1-yl)-[1,1'-biphenyl]-4-yl)-1H-benzo[d]imidazole

Base Information

Chemical Name:1-(4'-methoxy-2,3,5,6-tetra(1H-pyrazol-1-yl)-[1,1'-biphenyl]-4-yl)-1H-benzo[d]imidazole
CAS No.:1610894-64-8
Molecular Formula:C₃₂H₂₄N₁₀O
Molecular Weight:564.609
Hs Code.:

Synonyms:1-(4'-methoxy-2,3,5,6-tetra(1H-pyrazol-1-yl)-[1,1'-biphenyl]-4-yl)-1H-benzo[d]imidazole

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Chemical Property of 1-(4'-methoxy-2,3,5,6-tetra(1H-pyrazol-1-yl)-[1,1'-biphenyl]-4-yl)-1H-benzo[d]imidazole

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Technology Process of 1-(4'-methoxy-2,3,5,6-tetra(1H-pyrazol-1-yl)-[1,1'-biphenyl]-4-yl)-1H-benzo[d]imidazole

There total 4 articles about 1-(4'-methoxy-2,3,5,6-tetra(1H-pyrazol-1-yl)-[1,1'-biphenyl]-4-yl)-1H-benzo[d]imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 288-13-1
NH-pyrazole

: 1610894-59-1
1-(2,3,5,6-tetrafluoro-4'-methoxybiphenyl-4-yl)-1H-benzo[d]imidazole

: 1610894-64-8
1-(4'-methoxy-2,3,5,6-tetra(1H-pyrazol-1-yl)-[1,1'-biphenyl]-4-yl)-1H-benzo[d]imidazole

Guidance literature:: With sodium t-butanolate; In N,N-dimethyl acetamide; at 20 ℃; for 1h;
DOI:10.1021/ol5012554

Reference yield:

: 51-17-2,79351-71-6
benzoimidazole

: 1610894-64-8
1-(4'-methoxy-2,3,5,6-tetra(1H-pyrazol-1-yl)-[1,1'-biphenyl]-4-yl)-1H-benzo[d]imidazole

Guidance literature:: Multi-step reaction with 3 steps

1: sodium t-butanolate / N,N-dimethyl acetamide / 1 h / -10 - 20 °C

2: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium carbonate / N,N-dimethyl acetamide / 0.25 h / 160 °C / Microwave irradiation; Inert atmosphere

3: sodium t-butanolate / N,N-dimethyl acetamide / 1 h / 20 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; potassium carbonate; sodium t-butanolate; In N,N-dimethyl acetamide; 2: |Suzuki Coupling;
DOI:10.1021/ol5012554

Reference yield:

: 1610894-54-6
1-(4-bromo-2,3,5,6-tetrafluorophenyl)-1H-benzo[d]imidazole

: 1610894-64-8
1-(4'-methoxy-2,3,5,6-tetra(1H-pyrazol-1-yl)-[1,1'-biphenyl]-4-yl)-1H-benzo[d]imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; triphenylphosphine; caesium carbonate / N,N-dimethyl acetamide / 1 h / 130 °C / Microwave irradiation; Inert atmosphere

2: sodium t-butanolate / N,N-dimethyl acetamide / 1 h / 20 °C

With palladium diacetate; caesium carbonate; triphenylphosphine; sodium t-butanolate; In N,N-dimethyl acetamide; 1: |Suzuki Coupling;
DOI:10.1021/ol5012554