(+/-)-1-p-toluenesulfonyl-5-tert-butoxycarbonylamino-1,3-cyclohexadiene

Base Information

• Chemical Name: (+/-)-1-p-toluenesulfonyl-5-tert-butoxycarbonylamino-1,3-cyclohexadiene
• CAS No.: 155148-88-2
• Molecular Formula: C₁₈H₂₃NO₄S
• Molecular Weight: 349.451
• Mol file: 155148-88-2.mol

Synonyms:(+/-)-1-p-toluenesulfonyl-5-tert-butoxycarbonylamino-1,3-cyclohexadiene

Chemical Property of (+/-)-1-p-toluenesulfonyl-5-tert-butoxycarbonylamino-1,3-cyclohexadiene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (+/-)-1-p-toluenesulfonyl-5-tert-butoxycarbonylamino-1,3-cyclohexadiene

There total 1 articles about (+/-)-1-p-toluenesulfonyl-5-tert-butoxycarbonylamino-1,3-cyclohexadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

(+/-)-2-p-toluenesulfonyl-7-tert-butoxycarbonyl-7-azabicyclo[2.2.1]hept-5-ene → (+/-)-1-p-toluenesulfonyl-5-tert-butoxycarbonylamino-1,3-cyclohexadiene (155148-88-2)

Guidance literature:

With lithium hexamethyldisilazane; In tetrahydrofuran; at -20 ℃; for 0.333333h;

DOI:10.1021/jo971907r

Reference yield: 91.0%

(+/-)-1-p-toluenesulfonyl-5-tert-butoxycarbonylamino-1,3-cyclohexadiene (155148-88-2) → [(1R,2R,6S)-4-(Toluene-4-sulfonyl)-7-oxa-bicyclo[4.1.0]hept-4-en-2-yl]-carbamic acid tert-butyl ester

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 16h; Ambient temperature;

DOI:10.1021/jo971907r

Reference yield: 85.0%

di-tert-butyl dicarbonate (24424-99-5) + (+/-)-1-p-toluenesulfonyl-5-tert-butoxycarbonylamino-1,3-cyclohexadiene (155148-88-2) → N,N-bis-tert-butoxy-(+/-)-1-p-toluenesulfonyl-5-aminocyclohex-1,3-diene (155148-89-3)

Guidance literature:

dmap; In acetonitrile;

DOI:10.1016/0040-4039(94)88307-6

Downstream raw materials:

N,N-bis-tert-butoxy-(+/-)-1-p-toluenesulfonyl-5-aminocyclohex-1,3-diene

(+/-)-Tetraacetyl-konduramin-A-1

(1SR,2SR,3RS,6SR)-6-aminocyclohex-4-ene-1,2,3-triol

r-1-Acetamido-2-cyclohexen-c-4,t-5,c-6-triyltriacetat