C₃₂H₃₇NO₄

Base Information

• Chemical Name: C₃₂H₃₇NO₄
• CAS No.: 1245791-51-8
• Molecular Formula: C₃₂H₃₇NO₄
• Molecular Weight: 499.65
• Mol file: 1245791-51-8.mol

Synonyms:C₃₂H₃₇NO₄

Chemical Property of C₃₂H₃₇NO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₃₂H₃₇NO₄

There total 7 articles about C₃₂H₃₇NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C48H55NO4Si → C32H37NO4 (1245791-51-8)

Guidance literature:

With zinc(II) tetrafluoroborate hexahydrate; In tetrahydrofuran; water; at 50 ℃; for 72h;

DOI:10.1039/c6cp01058j

Reference yield: 90.0%

4'-hydroxy-2,2'-dimethyl-1,1'-biphenyl-4-carbonitrile (1245791-49-4) + 4-[(10-hydroxydecyl)oxy]benzoic acid (139298-69-4) → C32H37NO4 (1245791-51-8)

Guidance literature:

With 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/ic101220v

Reference yield:

C33H44O4Si → C32H37NO4 (1245791-51-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 4-(dimethylamino)pyridinium tosylate; dicyclohexyl-carbodiimide; 4-pyrrolidin-1-ylpyridine / dichloromethane / 48 h / 0 - 20 °C

2: zinc(II) tetrafluoroborate hexahydrate / tetrahydrofuran; water / 72 h / 50 °C

With zinc(II) tetrafluoroborate hexahydrate; 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; In tetrahydrofuran; dichloromethane; water;

DOI:10.1039/c6cp01058j

upstream raw materials:

4'-hydroxy-2,2'-dimethyl-1,1'-biphenyl-4-carbonitrile

4-[(10-hydroxydecyl)oxy]benzoic acid

1-bromo-10-decanol

4-hydroxy-benzaldehyde

Downstream raw materials:

C₄₀H₄₁NO₆