[methoxy-13C,D₃,amido-13C] 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoic acid

Base Information

• Chemical Name: [methoxy-13C,D₃,amido-13C] 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoic acid
• CAS No.: 1130037-39-6
• Molecular Formula: C₁₅H₁₁ClFNO₄
• Molecular Weight: 328.662

Synonyms:[methoxy-13C,D₃,amido-13C] 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoic acid

Chemical Property of [methoxy-13C,D₃,amido-13C] 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoic acid

Chemical Property:

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Technology Process of [methoxy-13C,D₃,amido-13C] 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoic acid

There total 1 articles about [methoxy-13C,D₃,amido-13C] 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

[methoxy-13C,D3,imido-13C]methyl 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoate (1130037-37-4) → [methoxy-13C,D3,amido-13C] 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoic acid (1130037-39-6)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 5h;

DOI:10.1002/jlcr.1515

Reference yield:

[methoxy-13C,D3,amido-13C] 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoic acid (1130037-39-6) → [methoxy-13C,D3,amido-13C] 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoyl chloride (1130037-41-0)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; In toluene; at 97 ℃; for 1.66667h;

DOI:10.1002/jlcr.1515

upstream raw materials:

[methoxy-13C,D₃,imido-13C]methyl 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoate

Downstream raw materials:

[methoxy-13C,D₃,amido-13C] 4-(2-chloro-5-fluorobenzoylamino)-3-methoxybenzoyl chloride

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