C₄₄H₂₈

Base Information

Chemical Name:C₄₄H₂₈
CAS No.:1062556-20-0
Molecular Formula:C₄₄H₂₈
Molecular Weight:556.706
Hs Code.:

Synonyms:C₄₄H₂₈

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₄H₂₈

Chemical Property:

Purity/Quality:

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Technology Process of C₄₄H₂₈

There total 3 articles about C₄₄H₂₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100622-34-2
anthracene-9-boronic acid

: 1062556-20-0
C₄₄H₂₈

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 24 h / 120 °C

2: N-Bromosuccinimide / dichloromethane / 24 h / 25 °C / Inert atmosphere

3: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 4 h / 120 °C

With N-Bromosuccinimide; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; dichloromethane; water; toluene;

Reference yield:

: 1564-64-3
9-Bromoanthracene

: 1062556-20-0
C₄₄H₂₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C / Inert atmosphere

1.2: 20 °C

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 24 h / 120 °C

3.1: N-Bromosuccinimide / dichloromethane / 24 h / 25 °C / Inert atmosphere

4.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 4 h / 120 °C

With N-Bromosuccinimide; n-butyllithium; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; toluene;

Reference yield:

: 1062556-17-5
C₃₈H₂₄

: 1062556-20-0
C₄₄H₂₈

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / dichloromethane / 24 h / 25 °C / Inert atmosphere

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 4 h / 120 °C

With N-Bromosuccinimide; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; dichloromethane; water; toluene;