N-<2-(6'-bromo-2',3'-dimethoxyphenyl)-1-(3,4-methylenedioxyphenyl)ethyl>aminoacetaldehyde diethyl acetal

Base Information

Chemical Name:N-<2-(6'-bromo-2',3'-dimethoxyphenyl)-1-(3,4-methylenedioxyphenyl)ethyl>aminoacetaldehyde diethyl acetal
CAS No.:107290-32-4
Molecular Formula:C₂₃H₃₀BrNO₆
Molecular Weight:496.398
Hs Code.:

Synonyms:N-<2-(6'-bromo-2',3'-dimethoxyphenyl)-1-(3,4-methylenedioxyphenyl)ethyl>aminoacetaldehyde diethyl acetal

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Chemical Property of N-<2-(6'-bromo-2',3'-dimethoxyphenyl)-1-(3,4-methylenedioxyphenyl)ethyl>aminoacetaldehyde diethyl acetal

Chemical Property:

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Technology Process of N-<2-(6'-bromo-2',3'-dimethoxyphenyl)-1-(3,4-methylenedioxyphenyl)ethyl>aminoacetaldehyde diethyl acetal

There total 9 articles about N-<2-(6'-bromo-2',3'-dimethoxyphenyl)-1-(3,4-methylenedioxyphenyl)ethyl>aminoacetaldehyde diethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107290-31-3
[1-Benzo[1,3]dioxol-5-yl-2-(6-bromo-2,3-dimethoxy-phenyl)-eth-(E)-ylidene]-(2,2-diethoxy-ethyl)-amine

: 107290-32-4
N-<2-(6'-bromo-2',3'-dimethoxyphenyl)-1-(3,4-methylenedioxyphenyl)ethyl>aminoacetaldehyde diethyl acetal

Guidance literature:: With sodium tetrahydroborate; In methanol; for 3h; Ambient temperature;

Reference yield:

: 274-09-9
Methylenedioxybenzene

: 107290-32-4
N-<2-(6'-bromo-2',3'-dimethoxyphenyl)-1-(3,4-methylenedioxyphenyl)ethyl>aminoacetaldehyde diethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 60.7 percent / stannic chloride / CH₂Cl₂ / 2 h / -50 °C

2: titanium tetrachloride / benzene / 30 min, 0-5 degC, 40 h, reflux

3: NaBH₄ / methanol / 3 h / Ambient temperature

With sodium tetrahydroborate; titanium tetrachloride; tin(IV) chloride; In methanol; dichloromethane; benzene;

Reference yield:

: 53811-50-0
6-bromo-2,3-dimethoxybenzaldehyde

: 107290-32-4
N-<2-(6'-bromo-2',3'-dimethoxyphenyl)-1-(3,4-methylenedioxyphenyl)ethyl>aminoacetaldehyde diethyl acetal

Guidance literature:: Multi-step reaction with 8 steps

1: 83.8 percent / NaBH₄ / tetrahydrofuran / 1 h / Ambient temperature

2: 94.1 percent / thionyl chloride, N,N-dimethylaniline / benzene / 1 h, room temperature, 30 min, 100 degC

3: 91.8 percent / dimethylsulfoxide / 1 h / 40 - 50 °C

4: 63.8 percent / 40percent KOH / H₂O; bis-(2-hydroxy-ethyl) ether / 8 h / Heating

5: thionyl chloride

6: 60.7 percent / stannic chloride / CH₂Cl₂ / 2 h / -50 °C

7: titanium tetrachloride / benzene / 30 min, 0-5 degC, 40 h, reflux

8: NaBH₄ / methanol / 3 h / Ambient temperature

With potassium hydroxide; sodium tetrahydroborate; thionyl chloride; titanium tetrachloride; tin(IV) chloride; N,N-dimethyl-aniline; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; diethylene glycol; benzene;