N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine

Base Information

Chemical Name:N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine
CAS No.:136670-08-1
Molecular Formula:C₂₆H₂₈N₄O₃
Molecular Weight:444.533
Hs Code.:

Synonyms:N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine

Chemical Property:

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Technology Process of N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine

There total 5 articles about N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 136670-07-0
N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine ethyl ester

: 136670-08-1
N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine

Guidance literature:: With potassium hydroxide; In ethanol; at 50 ℃; for 3h;
DOI:10.1016/S0223-5234(99)80045-2

Reference yield:

: 5878-41-1
lysergamine

: 136670-08-1
N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine

Guidance literature:: Multi-step reaction with 4 steps

1: 77 percent / dimethylformamide / 3 h / Ambient temperature

2: 79 percent / KOH / ethanol / 3 h / Ambient temperature

3: 1) 1,1'-carbonyldiimidazole / 1) dioxane, reflux, 15 min, 2) dioxane, reflux, 3 h

4: 77 percent / KOH / ethanol / 3 h / 50 °C

With potassium hydroxide; 1,1'-carbonyldiimidazole; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/S0223-5234(99)80045-2

Reference yield:

: 62-53-3
aniline

: 136670-08-1
N-<(9,10-didehydro-6-methylergolin-8β-yl)methyl>-N-(phenylcarbamoylmethyl)-glycine

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 1,1'-carbonyldiimidazole / 1) dioxane, reflux, 15 min, 2) dioxane, reflux, 3 h

2: 77 percent / KOH / ethanol / 3 h / 50 °C

With potassium hydroxide; 1,1'-carbonyldiimidazole; In ethanol;
DOI:10.1016/S0223-5234(99)80045-2