1,3-dimethyl-5-[1-(4-methoxyphenyl)-3-oxo-3-phenylpropyl]pyrimidine-2,4,6(1H,3H,5H)-trione

Base Information

• Chemical Name: 1,3-dimethyl-5-[1-(4-methoxyphenyl)-3-oxo-3-phenylpropyl]pyrimidine-2,4,6(1H,3H,5H)-trione
• CAS No.: 959833-62-6
• Molecular Formula: C₂₂H₂₂N₂O₅
• Molecular Weight: 394.427

Synonyms:1,3-dimethyl-5-[1-(4-methoxyphenyl)-3-oxo-3-phenylpropyl]pyrimidine-2,4,6(1H,3H,5H)-trione

Chemical Property of 1,3-dimethyl-5-[1-(4-methoxyphenyl)-3-oxo-3-phenylpropyl]pyrimidine-2,4,6(1H,3H,5H)-trione

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Technology Process of 1,3-dimethyl-5-[1-(4-methoxyphenyl)-3-oxo-3-phenylpropyl]pyrimidine-2,4,6(1H,3H,5H)-trione

There total 3 articles about 1,3-dimethyl-5-[1-(4-methoxyphenyl)-3-oxo-3-phenylpropyl]pyrimidine-2,4,6(1H,3H,5H)-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

1,3-dimethylbarbituric acid (769-42-6) + 3-(4-methoxyphenyl)-1-phenylprop-2-en-1-one (959-33-1) → 1,3-dimethyl-5-[1-(4-methoxyphenyl)-3-oxo-3-phenylpropyl]pyrimidine-2,4,6(1H,3H,5H)-trione (959833-62-6)

Guidance literature:

With diethylamine; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1016/j.tetlet.2015.10.108

Reference yield: 87.0%

1-styrenyloxytrimethylsilane (13735-81-4) + 5-(4-methoxy-benzylidene)-1,3-dimethyl-pyrimidine-2,4,6-trione (57270-82-3) → 1,3-dimethyl-5-[1-(4-methoxyphenyl)-3-oxo-3-phenylpropyl]pyrimidine-2,4,6(1H,3H,5H)-trione (959833-62-6)

Guidance literature:

In dimethyl sulfoxide; at 20 ℃; for 24h;

DOI:10.1021/jo071273g

Reference yield: 70.0%

1,3-dimethylbarbituric acid (769-42-6) + trans-4-methoxychalcone (22252-15-9) → 1,3-dimethyl-5-[1-(4-methoxyphenyl)-3-oxo-3-phenylpropyl]pyrimidine-2,4,6(1H,3H,5H)-trione (959833-62-6)

Guidance literature:

With triethylamine; In methanol; at 80 - 85 ℃; for 4h;

DOI:10.1016/0040-4020(96)00537-6

upstream raw materials:

1,3-dimethylbarbituric acid

trans-4-methoxychalcone

1-styrenyloxytrimethylsilane

5-(4-methoxy-benzylidene)-1,3-dimethyl-pyrimidine-2,4,6-trione

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