N-benzyloxycarbonyl-2-aminoethyl-O-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-O-(3-O-benzyl-α-L-idopyranosyluronic acid)(1->4)-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-3-O-benzyl-α-L-idopyranosiduronic acid

Base Information

Chemical Name:N-benzyloxycarbonyl-2-aminoethyl-O-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-O-(3-O-benzyl-α-L-idopyranosyluronic acid)(1->4)-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-3-O-benzyl-α-L-idopyranosiduronic acid
CAS No.:1266234-52-9
Molecular Formula:C₆₉H₇₇N₇O₂₃
Molecular Weight:1372.4
Hs Code.:

N-benzyloxycarbonyl-2-aminoethyl-O-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-O-(3-O-benzyl-α-L-idopyranosyluronic acid)(1->4)-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-3-O-benzyl-α-L-idopyranosiduronic acid

Synonyms:N-benzyloxycarbonyl-2-aminoethyl-O-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-O-(3-O-benzyl-α-L-idopyranosyluronic acid)(1->4)-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-3-O-benzyl-α-L-idopyranosiduronic acid

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Chemical Property of N-benzyloxycarbonyl-2-aminoethyl-O-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-O-(3-O-benzyl-α-L-idopyranosyluronic acid)(1->4)-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-3-O-benzyl-α-L-idopyranosiduronic acid

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Technology Process of N-benzyloxycarbonyl-2-aminoethyl-O-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-O-(3-O-benzyl-α-L-idopyranosyluronic acid)(1->4)-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-3-O-benzyl-α-L-idopyranosiduronic acid

There total 1 articles about N-benzyloxycarbonyl-2-aminoethyl-O-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-O-(3-O-benzyl-α-L-idopyranosyluronic acid)(1->4)-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-3-O-benzyl-α-L-idopyranosiduronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1364662-77-0
N-benzyloxycarbonyl-2-aminoethyl-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-O-(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)(1->4)-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosiduronate

: 1266234-52-9
N-benzyloxycarbonyl-2-aminoethyl-O-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-O-(3-O-benzyl-α-L-idopyranosyluronic acid)(1->4)-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-3-O-benzyl-α-L-idopyranosiduronic acid

Guidance literature:: N-benzyloxycarbonyl-2-aminoethyl-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-O-(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)(1->4)-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosiduronate; With dihydrogen peroxide; lithium hydroxide; In tetrahydrofuran; at -5 - 20 ℃; for 20h;

With sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃;

With hydrogenchloride; In tetrahydrofuran; methanol; water;
DOI:10.1039/c2ob06607f

Reference yield: 95.0%

: 1266234-52-9
N-benzyloxycarbonyl-2-aminoethyl-O-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-O-(3-O-benzyl-α-L-idopyranosyluronic acid)(1->4)-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-3-O-benzyl-α-L-idopyranosiduronic acid

: C₆₉H₇₁N₇O₃₅S₄^(6-)*6Na⁽¹⁺⁾

Guidance literature:: With sulfur trioxide trimethylamine complex; In N,N-dimethyl-formamide; at 100 ℃; for 0.5h; Microwave irradiation; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.11.094

Reference yield: 95.0%

: 1266234-52-9
N-benzyloxycarbonyl-2-aminoethyl-O-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-O-(3-O-benzyl-α-L-idopyranosyluronic acid)(1->4)-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-3-O-benzyl-α-L-idopyranosiduronic acid

: 121-44-8
triethylamine

: N-benzyloxycarbonyl-2-aminoethyl-O-(2-azido-3,4-di-O-benzyl-2-deoxy-6-O-sulfo-α-D-glucopyranosyl)(1->4)-O-(3-O-benzyl-2-O-sulfo-α-L-idopyranosyluronic acid)(1->4)-O-(2-azido-3-O-benzyl-2-deoxy-6-O-sulfo-α-D-glucopyranosyl)(1->4)-3-O-benzyl-2-O-sulfo-α-L-idopyranosiduronic acid triethylammonium salt

Guidance literature:: N-benzyloxycarbonyl-2-aminoethyl-O-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-O-(3-O-benzyl-α-L-idopyranosyluronic acid)(1->4)-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)-3-O-benzyl-α-L-idopyranosiduronic acid; With sulfur trioxide trimethylamine complex; In N,N-dimethyl-formamide; at 100 ℃; for 0.25h; Microwave irradiation;

triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide; Inert atmosphere;
DOI:10.1039/c2ob06607f