ethyl 2-(2,4,6-trimethylphenyl)cyanoacetate

Base Information

Chemical Name:ethyl 2-(2,4,6-trimethylphenyl)cyanoacetate
CAS No.:34404-82-5
Molecular Formula:C₁₄H₁₇NO₂
Molecular Weight:231.294
Hs Code.:

Synonyms:ethyl 2-(2,4,6-trimethylphenyl)cyanoacetate

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Chemical Property of ethyl 2-(2,4,6-trimethylphenyl)cyanoacetate

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Technology Process of ethyl 2-(2,4,6-trimethylphenyl)cyanoacetate

There total 4 articles about ethyl 2-(2,4,6-trimethylphenyl)cyanoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1667-04-5
2-bromomesitylene

: 105-56-6
ethyl 2-cyanoacetate

: 34404-82-5
ethyl 2-(2,4,6-trimethylphenyl)cyanoacetate

Guidance literature:: 2-bromomesitylene; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; bis(proazaphosphatrane); potassium tert-butylate; In toluene; at 20 ℃; for 0.333333h; Schlenk technique; Inert atmosphere;

ethyl 2-cyanoacetate; In toluene; at 80 ℃; for 4h; Inert atmosphere; Schlenk technique;
DOI:10.1002/ejoc.201402466

Reference yield: 89.0%

: 576-83-0
2,4,6-trimethylphenyl bromide

: 105-56-6
ethyl 2-cyanoacetate

: 34404-82-5
ethyl 2-(2,4,6-trimethylphenyl)cyanoacetate

Guidance literature:: With P(i-BuNCH₂CH₂)3N; potassium tert-butylate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In toluene; at 90 ℃; for 5h;
DOI:10.1021/jo034779h

Reference yield: 17.0%

: 34404-82-5
ethyl 2-(2,4,6-trimethylphenyl)cyanoacetate

Guidance literature:: With tri-tert-butyl phosphine; sodium phosphate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In toluene; at 90 ℃; for 20h; Inert atmosphere; Sealed tube;