2-hydroxy-5-chlorobenzyl mercaptan

Base Information

Chemical Name:2-hydroxy-5-chlorobenzyl mercaptan
CAS No.:118143-41-2
Molecular Formula:C₇H₇ClOS
Molecular Weight:174.651
Hs Code.:

Synonyms:2-hydroxy-5-chlorobenzyl mercaptan

Suppliers and Price of 2-hydroxy-5-chlorobenzyl mercaptan

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-hydroxy-5-chlorobenzyl mercaptan

Chemical Property:

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Technology Process of 2-hydroxy-5-chlorobenzyl mercaptan

There total 2 articles about 2-hydroxy-5-chlorobenzyl mercaptan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 6296-67-9
2-acetoxy-5-chlorobenzyl acetate

: 118143-41-2
2-hydroxy-5-chlorobenzyl mercaptan

Guidance literature:: With sodium hydrogensulfide; In methanol; for 2h; Heating;
DOI:10.1021/jo00268a020

Reference yield:

: 321-14-2
5-chloro-2-hydroxybenzoic acid

: 118143-41-2
2-hydroxy-5-chlorobenzyl mercaptan

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / LiAlH₄ / diethyl ether / 0.75 h / Heating

2: 97 percent / pyridine / 2 h / 25 °C

3: 91 percent / sodium hydrogen sulfide / methanol / 2 h / Heating

With pyridine; sodium hydrogensulfide; lithium aluminium tetrahydride; In methanol; diethyl ether;
DOI:10.1021/jo00268a020