3-Azido-5-ethyl-6-phenylphenanthridinium chloride

Base Information

• Chemical Name: 3-Azido-5-ethyl-6-phenylphenanthridinium chloride
• CAS No.: 74920-70-0
• Molecular Formula: C₂₁H₁₇N₄*Cl
• Molecular Weight: 360.846
• Mol file: 74920-70-0.mol

Synonyms:

Chemical Property of 3-Azido-5-ethyl-6-phenylphenanthridinium chloride

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Azido-5-ethyl-6-phenylphenanthridinium chloride

There total 2 articles about 3-Azido-5-ethyl-6-phenylphenanthridinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethidium Bromide (1239-45-8) → 3-azido-5-ethyl-6-phenylphenanthridinium chloride (74920-70-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 24 percent / aq. HCl, 48percent hypophosphorous acid, sodium nitrite / H₂O / 0 °C

2: 1) aq. HCl, sodium nitrite 2) water, sodium azide / 1) 0 deg C, 5 min. 2) water, overnight

With hydrogenchloride; sodium azide; water; hypophosphorous acid; sodium nitrite; In water;

Reference yield:

3-amino-5-ethyl-6-phenylphenanthridinium chloride (74920-69-7) → 3-azido-5-ethyl-6-phenylphenanthridinium chloride (74920-70-0)

Guidance literature:

With hydrogenchloride; sodium azide; water; sodium nitrite; Yield given. Multistep reaction; 1) 0 deg C, 5 min. 2) water, overnight;

upstream raw materials:

3-amino-5-ethyl-6-phenylphenanthridinium chloride

ethidium Bromide

Refernces