N-<(1R,2S,3R,4S)-2-hydroxy-1,7,7-trimethylbucyclohept-3-yl>-3-(phenylthio)-2-<(phenylthio)methyl>propanamide

Base Information Edit

Chemical Name:N-<(1R,2S,3R,4S)-2-hydroxy-1,7,7-trimethylbucyclohept-3-yl>-3-(phenylthio)-2-<(phenylthio)methyl>propanamide
CAS No.:116407-55-7
Molecular Formula:C₂₆H₃₃NO₂S₂
Molecular Weight:455.686
Hs Code.:
Mol file:116407-55-7.mol

Synonyms:N-<(1R,2S,3R,4S)-2-hydroxy-1,7,7-trimethylbucyclohept-3-yl>-3-(phenylthio)-2-<(phenylthio)methyl>propanamide

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Chemical Property of N-<(1R,2S,3R,4S)-2-hydroxy-1,7,7-trimethylbucyclohept-3-yl>-3-(phenylthio)-2-<(phenylthio)methyl>propanamide Edit

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Technology Process of N-<(1R,2S,3R,4S)-2-hydroxy-1,7,7-trimethylbucyclohept-3-yl>-3-(phenylthio)-2-<(phenylthio)methyl>propanamide

There total 2 articles about N-<(1R,2S,3R,4S)-2-hydroxy-1,7,7-trimethylbucyclohept-3-yl>-3-(phenylthio)-2-<(phenylthio)methyl>propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 41719-73-7
(2S)-3-exo-aminoisoborneol

: 116407-54-6
3-(phenylthio)-2-<(phenylthio)methyl>propionyl chloride

: 116407-55-7
N-<(1R,2S,3R,4S)-2-hydroxy-1,7,7-trimethylbucyclohept-3-yl>-3-(phenylthio)-2-<(phenylthio)methyl>propanamide

Guidance literature:: With triethylamine; In tetrahydrofuran; 0 deg C -> room temperature;
DOI:10.1021/ja00229a038

Reference yield:

: 92806-66-1
3-(phenylthio)-2-<(phenylthio)methyl>propionic acid

: 116407-55-7
N-<(1R,2S,3R,4S)-2-hydroxy-1,7,7-trimethylbucyclohept-3-yl>-3-(phenylthio)-2-<(phenylthio)methyl>propanamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / benzene

2: 43 percent / triethylamine / tetrahydrofuran / 0 deg C -> room temperature

With thionyl chloride; triethylamine; In tetrahydrofuran; benzene;
DOI:10.1021/ja00229a038