“(3-benzyloxy-7-methoxy-naphthalene-2-yl-amino)-acetic acid-methyl ester”

Base Information

Chemical Name:“(3-benzyloxy-7-methoxy-naphthalene-2-yl-amino)-acetic acid-methyl ester”
CAS No.:1092455-21-4
Molecular Formula:C₂₁H₂₁NO₄
Molecular Weight:351.402
Hs Code.:

Synonyms:“(3-benzyloxy-7-methoxy-naphthalene-2-yl-amino)-acetic acid-methyl ester”

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Chemical Property of “(3-benzyloxy-7-methoxy-naphthalene-2-yl-amino)-acetic acid-methyl ester”

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Technology Process of “(3-benzyloxy-7-methoxy-naphthalene-2-yl-amino)-acetic acid-methyl ester”

There total 4 articles about “(3-benzyloxy-7-methoxy-naphthalene-2-yl-amino)-acetic acid-methyl ester” which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1092455-20-3
3-benzyloxy-7-methoxy-naphthalene-2-yl-amine

: 96-32-2
bromoacetic acid methyl ester

: 1092455-21-4
“(3-benzyloxy-7-methoxy-naphthalene-2-yl-amino)-acetic acid-methyl ester”

Guidance literature:: With water; potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 1.16667h;

Reference yield:

: 1092455-17-8
3-benzyloxy-7-methoxynaphthalene-2-carboxylic acid benzyl ester

: 1092455-21-4
“(3-benzyloxy-7-methoxy-naphthalene-2-yl-amino)-acetic acid-methyl ester”

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol; sodium hydroxide / 20 h / 20 - 60 °C

2: triethylamine; diphenyl phosphoryl azide / toluene / 18 h / 20 - 100 °C

3: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C

4: potassium carbonate / N,N-dimethyl-formamide / 18 h / 60 °C

With ethanol; diphenyl phosphoryl azide; potassium carbonate; triethylamine; trifluoroacetic acid; sodium hydroxide; In dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1092455-18-9
3-(benzyloxy)-7-methoxynaphthalene-2-carboxylic acid

: 1092455-21-4
“(3-benzyloxy-7-methoxy-naphthalene-2-yl-amino)-acetic acid-methyl ester”

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; diphenyl phosphoryl azide / toluene / 18 h / 20 - 100 °C

2: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 18 h / 60 °C

With diphenyl phosphoryl azide; potassium carbonate; triethylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide; toluene;