2-O-(2-O-methoxyacetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-6-O-(2,3,4-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

Base Information

Chemical Name:2-O-(2-O-methoxyacetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-6-O-(2,3,4-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol
CAS No.:1391099-46-9
Molecular Formula:C₉₁H₉₆O₁₈
Molecular Weight:1477.75
Hs Code.:

Synonyms:2-O-(2-O-methoxyacetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-6-O-(2,3,4-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

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Chemical Property of 2-O-(2-O-methoxyacetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-6-O-(2,3,4-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

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Technology Process of 2-O-(2-O-methoxyacetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-6-O-(2,3,4-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

There total 1 articles about 2-O-(2-O-methoxyacetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-6-O-(2,3,4-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1391099-44-7
1-O-allyl-2-O-(2-O-methoxyacetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-6-O-(2,3,4-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

: 1391099-46-9
2-O-(2-O-methoxyacetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-6-O-(2,3,4-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

Guidance literature:: 1-O-allyl-2-O-(2-O-methoxyacetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-6-O-(2,3,4-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol; With (1,5-cyclooctadiene)[bis(methyldiphenylphosphine)]iridium(I) hexafluorophosphate; hydrogen; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;

With mercury dichloride; mercury(II) oxide; In water; acetone; for 1.5h; Reflux;
DOI:10.1021/jo301189y

Reference yield:

: triethylammonium 1-O-((R)-10-methyloctadecanoyl)-2-O-hexadecanoyl-sn-glycero-3-H-phosphonate

: 1391099-46-9
2-O-(2-O-methoxyacetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-6-O-(2,3,4-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

: C₁₂₉H₁₆₉O₂₅P

Guidance literature:: triethylammonium 1-O-((R)-10-methyloctadecanoyl)-2-O-hexadecanoyl-sn-glycero-3-H-phosphonate; 2-O-(2-O-methoxyacetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-6-O-(2,3,4-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol; With pyridine; pivaloyl chloride; at 20 ℃; for 2h;

With pyridine; iodine; In water; for 1h;

In methanol; dichloromethane;
DOI:10.1021/jo301189y