methyl (3R)-3-[(3R)-3-{(3R)-3-[(3R)-3-(benzyloxy)butanoyloxy]butanoyloxy}butanoyloxy]butanoate

Base Information

Chemical Name:methyl (3R)-3-[(3R)-3-{(3R)-3-[(3R)-3-(benzyloxy)butanoyloxy]butanoyloxy}butanoyloxy]butanoate
CAS No.:211113-98-3
Molecular Formula:C₂₄H₃₄O₉
Molecular Weight:466.529
Hs Code.:

Synonyms:methyl (3R)-3-[(3R)-3-{(3R)-3-[(3R)-3-(benzyloxy)butanoyloxy]butanoyloxy}butanoyloxy]butanoate

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Chemical Property of methyl (3R)-3-[(3R)-3-{(3R)-3-[(3R)-3-(benzyloxy)butanoyloxy]butanoyloxy}butanoyloxy]butanoate

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Technology Process of methyl (3R)-3-[(3R)-3-{(3R)-3-[(3R)-3-(benzyloxy)butanoyloxy]butanoyloxy}butanoyloxy]butanoate

There total 3 articles about methyl (3R)-3-[(3R)-3-{(3R)-3-[(3R)-3-(benzyloxy)butanoyloxy]butanoyloxy}butanoyloxy]butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 107265-56-5
(R)-3-(benzyloxy)butanoyl chloride

: 211113-97-2
methyl (3R)-3-[(3R)-3-{(3R)-3-hydroxybutanoyloxy}butanoyloxy}butanoate

: 211113-98-3
methyl (3R)-3-[(3R)-3-{(3R)-3-[(3R)-3-(benzyloxy)butanoyloxy]butanoyloxy}butanoyloxy]butanoate

Guidance literature:: With triethylamine; In chloroform; at 20 ℃; ice-water cooling;
DOI:10.1246/bcsj.71.1683

Reference yield:

: 195453-29-3
(R)-3-Hydroxy-butyric acid (R)-2-methoxycarbonyl-1-methyl-ethyl ester

: 211113-98-3
methyl (3R)-3-[(3R)-3-{(3R)-3-[(3R)-3-(benzyloxy)butanoyloxy]butanoyloxy}butanoyloxy]butanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 54 percent / triethylamine / CHCl₃ / 20 °C / ice-water cooling

2: 70 percent / hydrogen / Pd/C / ethanol / 20 °C

3: 86 percent / triethylamine / CHCl₃ / 20 °C / ice-water cooling

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; chloroform; 1: Esterification / 2: Hydrogenolysis / 3: Esterification;
DOI:10.1246/bcsj.71.1683

Reference yield:

: 211113-96-1
methyl (3R)-3-[(3R)-3-{(3R)-3-(benzyloxy)butanoyloxy}butanoyloxy]butanoate

: 211113-98-3
methyl (3R)-3-[(3R)-3-{(3R)-3-[(3R)-3-(benzyloxy)butanoyloxy]butanoyloxy}butanoyloxy]butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / hydrogen / Pd/C / ethanol / 20 °C

2: 86 percent / triethylamine / CHCl₃ / 20 °C / ice-water cooling

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; chloroform; 1: Hydrogenolysis / 2: Esterification;
DOI:10.1246/bcsj.71.1683