ethyl (methyl 2,3,4-tri-O-benzyl-6-amino-6,7-dideoxy-D-glycero-α-D-gluco-octopyranoside)uronate

Base Information

Chemical Name:ethyl (methyl 2,3,4-tri-O-benzyl-6-amino-6,7-dideoxy-D-glycero-α-D-gluco-octopyranoside)uronate
CAS No.:1646500-19-7
Molecular Formula:C₃₂H₃₉NO₇
Molecular Weight:549.664
Hs Code.:

Synonyms:ethyl (methyl 2,3,4-tri-O-benzyl-6-amino-6,7-dideoxy-D-glycero-α-D-gluco-octopyranoside)uronate

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Chemical Property of ethyl (methyl 2,3,4-tri-O-benzyl-6-amino-6,7-dideoxy-D-glycero-α-D-gluco-octopyranoside)uronate

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Technology Process of ethyl (methyl 2,3,4-tri-O-benzyl-6-amino-6,7-dideoxy-D-glycero-α-D-gluco-octopyranoside)uronate

There total 1 articles about ethyl (methyl 2,3,4-tri-O-benzyl-6-amino-6,7-dideoxy-D-glycero-α-D-gluco-octopyranoside)uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: ethyl (methyl 2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-gluco-oct-6-enopyranoside)uronate

: 1646500-16-4
ethyl (methyl 2,3,4-tri-O-benzyl-6-amino-6,7-dideoxy-L-glycero-α-D-gluco-octopyranoside)uronate

: 1646500-19-7
ethyl (methyl 2,3,4-tri-O-benzyl-6-amino-6,7-dideoxy-D-glycero-α-D-gluco-octopyranoside)uronate

Guidance literature:: With ammonia; In ethanol; at 23 ℃; for 24h; Overall yield = 88 %; Further stages; Sealed tube;
DOI:10.3762/bjoc.10.93

Reference yield: 90.0%

: 1646500-19-7
ethyl (methyl 2,3,4-tri-O-benzyl-6-amino-6,7-dideoxy-D-glycero-α-D-gluco-octopyranoside)uronate

: 1646500-20-0
C₃₀H₃₅NO₇

Guidance literature:: With lithium hydroxide monohydrate; In aq. phosphate buffer; ethanol; at 0 - 25 ℃; for 24h; pH=7; Further stages;
DOI:10.3762/bjoc.10.93

Reference yield:

: 1646500-19-7
ethyl (methyl 2,3,4-tri-O-benzyl-6-amino-6,7-dideoxy-D-glycero-α-D-gluco-octopyranoside)uronate

: 1646500-21-1
C₄₅H₄₅NO₉

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide monohydrate / ethanol; aq. phosphate buffer / 24 h / 0 - 25 °C / pH 7

2: sodium hydrogencarbonate / 1,4-dioxane; water / 0 - 20 °C

With lithium hydroxide monohydrate; sodium hydrogencarbonate; In 1,4-dioxane; aq. phosphate buffer; ethanol; water;
DOI:10.3762/bjoc.10.93