methyl 3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

Base Information

• Chemical Name: methyl 3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside
• CAS No.: 1144104-09-5
• Molecular Formula: C₄₁H₄₄O₁₁
• Molecular Weight: 712.794

Synonyms:methyl 3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

Chemical Property of methyl 3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

Chemical Property:

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Technology Process of methyl 3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

There total 1 articles about methyl 3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C44H46O11 → methyl 3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside (1144104-09-5)

Guidance literature:

With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetonitrile; at 20 ℃; for 2h;

DOI:10.1002/ejoc.200801024

Reference yield: 78.0%

methyl 3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside (1144104-09-5) + 2-O-acetyl-3,4,6-tri-O-benzyl-D-glucopyranosyl trichloroacetimidate (189182-66-9) → methyl 2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside (1144104-58-4)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -10 ℃; for 0.5h; stereoselective reaction; Inert atmosphere;

DOI:10.1002/ejoc.200801024

Reference yield:

C24H23F3O8S + methyl 3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside (1144104-09-5) → methyl 3-O-benzyl-4,6-O-benzylidene-2-O-(prop-2-ynyl)-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside (1144104-20-0) + C64H66O16

Guidance literature:

In dichloromethane; at -78 ℃; for 2h; optical yield given as %de; Inert atmosphere;

DOI:10.1002/ejoc.200801024

Downstream raw materials:

methyl 3-O-benzyl-4,6-O-benzylidene-2-O-(prop-2-ynyl)-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

methyl 2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

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