C₅₃H₈₈O₁₀Si₃

Base Information

Chemical Name:C₅₃H₈₈O₁₀Si₃
CAS No.:1264756-72-0
Molecular Formula:C₅₃H₈₈O₁₀Si₃
Molecular Weight:969.532
Hs Code.:

C<sub>53</sub>H<sub>88</sub>O<sub>10</sub>Si<sub>3</sub>

Synonyms:C₅₃H₈₈O₁₀Si₃

Suppliers and Price of C₅₃H₈₈O₁₀Si₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₃H₈₈O₁₀Si₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₃H₈₈O₁₀Si₃

There total 32 articles about C₅₃H₈₈O₁₀Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₃H₉₀O₁₀Si₃

: 1264756-72-0
C₅₃H₈₈O₁₀Si₃

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; at 0 - 20 ℃; Molecular sieve;
DOI:10.1016/j.tetlet.2010.11.127

Reference yield:

: 1264756-62-8
C₃₃H₄₀O₆

: 1264756-72-0
C₅₃H₈₈O₁₀Si₃

Guidance literature:: Multi-step reaction with 19 steps

1.1: diisobutylaluminium hydride / dichloromethane / -78 °C

2.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -40 °C / Molecular sieve

3.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 0 °C

4.1: sodium hexamethyldisilazane / tetrahydrofuran / 0 °C

5.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C

6.1: potassium tert-butylate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 20 °C

7.1: bis-(1,2-dimethylpropyl)borane / tetrahydrofuran / 0 - 20 °C

7.2: 20 °C

8.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 20 °C

9.1: diethyl ether / -78 °C

10.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 20 °C / Molecular sieve

11.1: di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine / diethyl ether / 0 °C

11.2: -78 °C

12.1: Dess-Martin periodane / dichloromethane; tert-butyl alcohol / 20 °C

13.1: pyridinium p-toluenesulfonate / methanol / 80 °C

14.1: 2,6-dimethylpyridine / N,N-dimethyl-formamide / 20 °C

15.1: sodium tetrahydroborate; cerium(III) chloride / methanol; dichloromethane / 0 °C

16.1: boron trifluoride tetrahydrofuran complex / tetrahydrofuran / 0 °C

16.2: 0 - 20 °C

17.1: 2,6-dimethylpyridine / dichloromethane / 20 °C

18.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0 °C

19.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 20 °C / Molecular sieve

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium hypochlorite; sodium tetrahydroborate; cerium(III) chloride; tetrapropylammonium perruthennate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; boron trifluoride tetrahydrofuran complex; diethyl (2R,3R)-tartrate; di-n-butylboryl trifluoromethanesulfonate; potassium tert-butylate; water; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; bis-(1,2-dimethylpropyl)borane; tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium bromide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 2.1: Sharpless asymmetric epoxidation / 4.1: Wittig reaction / 9.1: Grignard reaction / 12.1: Dess-Martin oxidation / 15.1: Luche reduction;
DOI:10.1016/j.tetlet.2010.11.127

Reference yield:

: 1264756-61-7
C₂₈H₃₄O₅

: 1264756-72-0
C₅₃H₈₈O₁₀Si₃

Guidance literature:: Multi-step reaction with 20 steps

1.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C

1.2: 20 °C

2.1: diisobutylaluminium hydride / dichloromethane / -78 °C

3.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -40 °C / Molecular sieve

4.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 0 °C

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 0 °C

6.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C

7.1: potassium tert-butylate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 20 °C

8.1: bis-(1,2-dimethylpropyl)borane / tetrahydrofuran / 0 - 20 °C

8.2: 20 °C

9.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 20 °C

10.1: diethyl ether / -78 °C

11.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 20 °C / Molecular sieve

12.1: di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine / diethyl ether / 0 °C

12.2: -78 °C

13.1: Dess-Martin periodane / dichloromethane; tert-butyl alcohol / 20 °C

14.1: pyridinium p-toluenesulfonate / methanol / 80 °C

15.1: 2,6-dimethylpyridine / N,N-dimethyl-formamide / 20 °C

16.1: sodium tetrahydroborate; cerium(III) chloride / methanol; dichloromethane / 0 °C

17.1: boron trifluoride tetrahydrofuran complex / tetrahydrofuran / 0 °C

17.2: 0 - 20 °C

18.1: 2,6-dimethylpyridine / dichloromethane / 20 °C

19.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0 °C

20.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 20 °C / Molecular sieve

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium hypochlorite; sodium tetrahydroborate; cerium(III) chloride; tetrapropylammonium perruthennate; oxalyl dichloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; boron trifluoride tetrahydrofuran complex; diethyl (2R,3R)-tartrate; di-n-butylboryl trifluoromethanesulfonate; potassium tert-butylate; water; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; bis-(1,2-dimethylpropyl)borane; tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium bromide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1.1: Swern oxidation / 1.2: Wittig reaction / 3.1: Sharpless asymmetric epoxidation / 5.1: Wittig reaction / 10.1: Grignard reaction / 13.1: Dess-Martin oxidation / 16.1: Luche reduction;
DOI:10.1016/j.tetlet.2010.11.127