2-acetyl-4-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo-[4.1.0]heptan-2-yl)-5-methoxy-1,3-phenylene diacetate

Base Information

Chemical Name:2-acetyl-4-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo-[4.1.0]heptan-2-yl)-5-methoxy-1,3-phenylene diacetate
CAS No.:1013913-56-8
Molecular Formula:C₂₃H₃₀O₇
Molecular Weight:418.487
Hs Code.:

Synonyms:2-acetyl-4-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo-[4.1.0]heptan-2-yl)-5-methoxy-1,3-phenylene diacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-acetyl-4-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo-[4.1.0]heptan-2-yl)-5-methoxy-1,3-phenylene diacetate

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Technology Process of 2-acetyl-4-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo-[4.1.0]heptan-2-yl)-5-methoxy-1,3-phenylene diacetate

There total 2 articles about 2-acetyl-4-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo-[4.1.0]heptan-2-yl)-5-methoxy-1,3-phenylene diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1013913-58-0
2-acetyl-4-((1R,6R)-6-isopropyl-3-methylcyclohex-2-enyl)-5-methoxy-1,3-phenylene diacetate

: 1013913-56-8
2-acetyl-4-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo-[4.1.0]heptan-2-yl)-5-methoxy-1,3-phenylene diacetate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 2h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo902567y

Reference yield:

: 1013913-58-0
2-acetyl-4-((1R,6R)-6-isopropyl-3-methylcyclohex-2-enyl)-5-methoxy-1,3-phenylene diacetate

: 1013913-56-8
2-acetyl-4-((1S,2S,3R,6R)-3-isopropyl-6-methyl-7-oxabicyclo-[4.1.0]heptan-2-yl)-5-methoxy-1,3-phenylene diacetate

: C₂₃H₃₀O₇

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 1h; Title compound not separated from byproducts.;
DOI:10.1055/s-2007-1000834