HP(CH₃)3C₆H₂CH₂PH(CH₃)3C₆H₂

Base Information

• Chemical Name: HP(CH₃)3C₆H₂CH₂PH(CH₃)3C₆H₂
• CAS No.: 118346-28-4
• Molecular Formula: C₁₉H₂₆P₂
• Molecular Weight: 316.363
• Mol file: 118346-28-4.mol

Synonyms:HP(CH₃)3C₆H₂CH₂PH(CH₃)3C₆H₂

Chemical Property of HP(CH₃)3C₆H₂CH₂PH(CH₃)3C₆H₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of HP(CH₃)3C₆H₂CH₂PH(CH₃)3C₆H₂

There total 3 articles about HP(CH₃)3C₆H₂CH₂PH(CH₃)3C₆H₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

CH2(P(Br)(C6H2(CH3)3))2 (118346-30-8,137935-82-1,137935-87-6) → HP(CH3)3C6H2CH2PH(CH3)3C6H2 (118346-28-4)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 16h; Ambient temperature;

Reference yield:

C19H24Cl2P2 (118346-29-5) → HP(CH3)3C6H2CH2PH(CH3)3C6H2 (118346-28-4)

Guidance literature:

Multi-step reaction with 2 steps

1: MgBr₂*Et₂O / diethyl ether / 16 h / 25 °C

2: 83 percent / LiAlH₄ / diethyl ether / 16 h / Ambient temperature

With lithium aluminium tetrahydride; magnesium bromide; In diethyl ether;

Reference yield:

2-mesitylmagnesium bromide (2633-66-1) → HP(CH3)3C6H2CH2PH(CH3)3C6H2 (118346-28-4)

Guidance literature:

Multi-step reaction with 3 steps

1: diethyl ether

2: MgBr₂*Et₂O / diethyl ether / 16 h / 25 °C

3: 83 percent / LiAlH₄ / diethyl ether / 16 h / Ambient temperature

With lithium aluminium tetrahydride; magnesium bromide; In diethyl ether;

upstream raw materials:

CH₂(P(Br)(C₆H₂(CH₃)3))2

C₁₉H₂₄Cl₂P₂

2-mesitylmagnesium bromide

Downstream raw materials:

Cu₈Cl₄((CH₃)3C₆H₂PCH₂P(CH₃)3C₆H₂)2(C₅H₅N)4(CH₃CN)

Cu₄Cl₃(HP(CH₃)3C₆H₂CH₂P(CH₃)3C₆H₂)(C₅H₅N)4

(CH₃)3SiP(CH₃)3C₆H₂CH₂PC₆H₂(CH₃)3Si(CH₃)3

Refernces