1D-1-O-(tert-butyldiphenylsilyl)-2,3,6-O-tris(methoxymethylene)-myo-inositol 4,5-bis(dibenzylphosphate)

Base Information

Chemical Name:1D-1-O-(tert-butyldiphenylsilyl)-2,3,6-O-tris(methoxymethylene)-myo-inositol 4,5-bis(dibenzylphosphate)
CAS No.:496808-68-5
Molecular Formula:C₅₆H₆₈O₁₅P₂Si
Molecular Weight:1071.18
Hs Code.:

Synonyms:1D-1-O-(tert-butyldiphenylsilyl)-2,3,6-O-tris(methoxymethylene)-myo-inositol 4,5-bis(dibenzylphosphate)

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Chemical Property of 1D-1-O-(tert-butyldiphenylsilyl)-2,3,6-O-tris(methoxymethylene)-myo-inositol 4,5-bis(dibenzylphosphate)

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Technology Process of 1D-1-O-(tert-butyldiphenylsilyl)-2,3,6-O-tris(methoxymethylene)-myo-inositol 4,5-bis(dibenzylphosphate)

There total 13 articles about 1D-1-O-(tert-butyldiphenylsilyl)-2,3,6-O-tris(methoxymethylene)-myo-inositol 4,5-bis(dibenzylphosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 496808-45-8
1D-4-O-benzoyl-1-O-(tert-butyldiphenylsilyl)-myo-inositol

: 496808-68-5
1D-1-O-(tert-butyldiphenylsilyl)-2,3,6-O-tris(methoxymethylene)-myo-inositol 4,5-bis(dibenzylphosphate)

Guidance literature:: Dibenzyl N,N-diisopropylphosphoramidite; 1D-4-O-benzoyl-1-O-(tert-butyldiphenylsilyl)-myo-inositol; With 1H-tetrazole; In acetonitrile; for 6h;

With 3-chloro-benzenecarboperoxoic acid; In chloroform; acetonitrile; at -20 - 20 ℃; Further stages.;
DOI:10.1021/jo0206418

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 496808-68-5
1D-1-O-(tert-butyldiphenylsilyl)-2,3,6-O-tris(methoxymethylene)-myo-inositol 4,5-bis(dibenzylphosphate)

Guidance literature:: Multi-step reaction with 4 steps

1.1: 88 percent / imidazole

2.1: 90 percent / HSCH₂CH₂OH; BF₃*Et₂O

3.1: pyridine

3.2: trifluoroacetic acid / H₂O; CHCl₃

4.1: tetrazole / acetonitrile / 6 h

4.2: 84 percent / 3-chloroperoxybenzoic acid / acetonitrile; CHCl₃ / -20 - 20 °C

With pyridine; 1H-imidazole; 1H-tetrazole; boron trifluoride diethyl etherate; 2-hydroxyethanethiol; In acetonitrile;
DOI:10.1021/jo0206418

Reference yield:

: 331679-26-6
2,3-O-(D-1,7,7-trimethylbicyclo[2.2.1]hept-6-ylidene)-D-myo-inositol

: 496808-68-5
1D-1-O-(tert-butyldiphenylsilyl)-2,3,6-O-tris(methoxymethylene)-myo-inositol 4,5-bis(dibenzylphosphate)

Guidance literature:: Multi-step reaction with 4 steps

1.1: 88 percent / imidazole

2.1: 90 percent / HSCH₂CH₂OH; BF₃*Et₂O

3.1: pyridine

3.2: trifluoroacetic acid / H₂O; CHCl₃

4.1: tetrazole / acetonitrile / 6 h

4.2: 84 percent / 3-chloroperoxybenzoic acid / acetonitrile; CHCl₃ / -20 - 20 °C

With pyridine; 1H-imidazole; 1H-tetrazole; boron trifluoride diethyl etherate; 2-hydroxyethanethiol; In acetonitrile;
DOI:10.1021/jo0206418