[(1R)-1-amino-2-(3-ethylphenyl)ethyl]boronic acid (+)-pinane-2,3-diyl diester trifluoroacetate

Base Information

Chemical Name:[(1R)-1-amino-2-(3-ethylphenyl)ethyl]boronic acid (+)-pinane-2,3-diyl diester trifluoroacetate
CAS No.:1444009-35-1
Molecular Formula:C₂HF₃O₂*C₂₀H₃₀BNO₂
Molecular Weight:441.299
Hs Code.:

Synonyms:[(1R)-1-amino-2-(3-ethylphenyl)ethyl]boronic acid (+)-pinane-2,3-diyl diester trifluoroacetate

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Chemical Property of [(1R)-1-amino-2-(3-ethylphenyl)ethyl]boronic acid (+)-pinane-2,3-diyl diester trifluoroacetate

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Technology Process of [(1R)-1-amino-2-(3-ethylphenyl)ethyl]boronic acid (+)-pinane-2,3-diyl diester trifluoroacetate

There total 7 articles about [(1R)-1-amino-2-(3-ethylphenyl)ethyl]boronic acid (+)-pinane-2,3-diyl diester trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1444010-72-3
N-((R)-2-(3-ethylphenyl)-1-((3aS,4S,6S,7aR)-3a,5,5-trimethylhexahydro-4,6-methanobenzo[d][1,3,2]dioxaborol-2-yl)ethyl)-1,1,1-trimethyl-N-(trimethylsilyl)silanamine

: 76-05-1
trifluoroacetic acid

: 1444009-35-1
[(1R)-1-amino-2-(3-ethylphenyl)ethyl]boronic acid (+)-pinane-2,3-diyl diester trifluoroacetate

Guidance literature:: In diethyl ether; at 0 ℃;

Reference yield:

: 216658-62-7
1-(bromomethyl)-3-ethylbenzene

: 1444009-35-1
[(1R)-1-amino-2-(3-ethylphenyl)ethyl]boronic acid (+)-pinane-2,3-diyl diester trifluoroacetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 12 h / 100 °C

2.1: diethyl ether / 12 h / 20 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -100 °C

3.2: -100 - 20 °C

4.1: tetrahydrofuran / -78 - 20 °C

5.1: diethyl ether / 0 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; diethyl ether; hexane;

Reference yield:

: 1444010-69-8
2-(3-ethylbenzyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1444009-35-1
[(1R)-1-amino-2-(3-ethylphenyl)ethyl]boronic acid (+)-pinane-2,3-diyl diester trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: diethyl ether / 12 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -100 °C

2.2: -100 - 20 °C

3.1: tetrahydrofuran / -78 - 20 °C

4.1: diethyl ether / 0 °C

With n-butyllithium; In tetrahydrofuran; diethyl ether; hexane;