1,2-Dihydro-2-cyclohexyldibenzoisoquinoline perchlorate

Base Information

Chemical Name:1,2-Dihydro-2-cyclohexyldibenzoisoquinoline perchlorate
CAS No.:107107-66-4
Molecular Formula:C₂₃H₂₃N*ClHO₄
Molecular Weight:413.901
Hs Code.:

1,2-Dihydro-2-cyclohexyldibenzo<f,h>isoquinoline perchlorate

Synonyms:1,2-Dihydro-2-cyclohexyldibenzoisoquinoline perchlorate

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Chemical Property of 1,2-Dihydro-2-cyclohexyldibenzoisoquinoline perchlorate

Chemical Property:

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Technology Process of 1,2-Dihydro-2-cyclohexyldibenzoisoquinoline perchlorate

There total 7 articles about 1,2-Dihydro-2-cyclohexyldibenzoisoquinoline perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 107107-57-3
1,2,3,4-Tetrahydro-2-cyclopropyldibenzoisoquinolin-4-ol

: 107107-66-4
1,2-Dihydro-2-cyclohexyldibenzoisoquinoline perchlorate

Guidance literature:: With perchloric acid; In acetic acid;
DOI:10.1002/jhet.5570230353

Reference yield:

: 37883-45-7
ethyl N-cyclohexylglycinate

: 107107-66-4
1,2-Dihydro-2-cyclohexyldibenzoisoquinoline perchlorate

Guidance literature:: Multi-step reaction with 6 steps

1: 40 percent / pyridine / benzene

2: 1.) triethyloxonium fluoroborate 2.) NaBH₄

3: 98 percent / conc. aq. HCl

4: 98 percent / polyphosphoric acid

5: 81 percent / NaBH₄

6: 80 percent / 70percent aq. HClO₄ / acetic acid

With pyridine; hydrogenchloride; sodium tetrahydroborate; perchloric acid; PPA; triethyloxonium fluoroborate; In acetic acid; benzene;
DOI:10.1002/jhet.5570230353

Reference yield:

: 107107-52-8
1,2,3,4-Tetrahydro-2-cyclopropyldibenzoisoquinolin-4-one

: 107107-66-4
1,2-Dihydro-2-cyclohexyldibenzoisoquinoline perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / NaBH₄

2: 80 percent / 70percent aq. HClO₄ / acetic acid

With sodium tetrahydroborate; perchloric acid; In acetic acid;
DOI:10.1002/jhet.5570230353