(2S,3R,3S)-4-(4-benzyloxy-3-methoxyphenyl)-2-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-methyl-4-butanolide

Base Information

Chemical Name:(2S,3R,3S)-4-(4-benzyloxy-3-methoxyphenyl)-2-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-methyl-4-butanolide
CAS No.:1204225-50-2
Molecular Formula:C₄₃H₅₄O₇Si
Molecular Weight:710.983
Hs Code.:

Synonyms:(2S,3R,3S)-4-(4-benzyloxy-3-methoxyphenyl)-2-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-methyl-4-butanolide

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Chemical Property of (2S,3R,3S)-4-(4-benzyloxy-3-methoxyphenyl)-2-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-methyl-4-butanolide

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Technology Process of (2S,3R,3S)-4-(4-benzyloxy-3-methoxyphenyl)-2-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-methyl-4-butanolide

There total 1 articles about (2S,3R,3S)-4-(4-benzyloxy-3-methoxyphenyl)-2-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-methyl-4-butanolide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: C₃₄H₃₄O₇

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 1204225-50-2
(2S,3R,3S)-4-(4-benzyloxy-3-methoxyphenyl)-2-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-methyl-4-butanolide

: (2S,3R,3S)-4-(4-benzyloxy-3-methoxyphenyl)-2-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-methyl-4-butanolide

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 20 ℃; Cooling with ice;
DOI:10.1271/bbb.90167

Reference yield: 77.0%

: 1204225-50-2
(2S,3R,3S)-4-(4-benzyloxy-3-methoxyphenyl)-2-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-methyl-4-butanolide

: 1204225-51-3
(1R,2R,3R,4S)-1,4-bis(4-benzyloxy-3-methoxyphenyl)-2-hydroxymethyl-3-methyl-1,4-butanediol

Guidance literature:: (2S,3R,3S)-4-(4-benzyloxy-3-methoxyphenyl)-2-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-3-methyl-4-butanolide; With diisobutylaluminium hydride; In toluene; at -70 ℃; for 3h;

With hydrogenchloride; In water; toluene; Further stages;
DOI:10.1271/bbb.90167