Technology Process of C16H18ClN3O5
There total 4 articles about C16H18ClN3O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrachloromethane; sodium hydrogencarbonate; triphenylphosphine;
for 12h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ammonium acetate / ethanol / Reflux
2: camphor-10-sulfonic acid / dichloromethane; methanol / 1.5 h / 0 - 20 °C
3: triphenylphosphine; sodium hydrogencarbonate; tetrachloromethane / 12 h / Reflux
With
tetrachloromethane; camphor-10-sulfonic acid; ammonium acetate; sodium hydrogencarbonate; triphenylphosphine;
In
methanol; ethanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: camphor-10-sulfonic acid / dichloromethane; methanol / 1.5 h / 0 - 20 °C
2: triphenylphosphine; sodium hydrogencarbonate; tetrachloromethane / 12 h / Reflux
With
tetrachloromethane; camphor-10-sulfonic acid; sodium hydrogencarbonate; triphenylphosphine;
In
methanol; dichloromethane;