3-Methoxy-16β-(N-p-nitrophenylaminomethyl)estra-1,3,5(10)-trien-17-β-ol

Base Information

Chemical Name:3-Methoxy-16β-(N-p-nitrophenylaminomethyl)estra-1,3,5(10)-trien-17-β-ol
CAS No.:145242-95-1
Molecular Formula:C₂₆H₃₂N₂O₄
Molecular Weight:436.551
Hs Code.:

Synonyms:3-Methoxy-16β-(N-p-nitrophenylaminomethyl)estra-1,3,5(10)-trien-17-β-ol

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Chemical Property of 3-Methoxy-16β-(N-p-nitrophenylaminomethyl)estra-1,3,5(10)-trien-17-β-ol

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Technology Process of 3-Methoxy-16β-(N-p-nitrophenylaminomethyl)estra-1,3,5(10)-trien-17-β-ol

There total 2 articles about 3-Methoxy-16β-(N-p-nitrophenylaminomethyl)estra-1,3,5(10)-trien-17-β-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 145243-01-2
Toluene-4-sulfonic acid (8R,9S,13S,14S,16R,17S)-3-methoxy-13-methyl-17-(4-nitro-phenylcarbamoyloxy)-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-16-ylmethyl ester

: 145242-95-1
3-Methoxy-16β-(N-p-nitrophenylaminomethyl)estra-1,3,5(10)-trien-17-β-ol

Guidance literature:: With sodium methylate; In methanol; for 3h; Heating;
DOI:10.1016/S0040-4020(01)85620-9

Reference yield:

: 3-Methoxy-16β-p-tolylsulfonyloxymethylestra-1,3,5(10)-trien-17β-ol O(17)-chlorocarbonic acid ester

: 145242-95-1
3-Methoxy-16β-(N-p-nitrophenylaminomethyl)estra-1,3,5(10)-trien-17-β-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent

2: 80 percent / NaOCH₃ / methanol / 3 h / Heating

With sodium methylate; In methanol;
DOI:10.1016/S0040-4020(01)85620-9