Technology Process of C32H38N4O5
There total 5 articles about C32H38N4O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
cyclohexa-1,4-diene; palladium 10% on activated carbon;
In
ethanol;
for 24h;
Reflux;
DOI:10.1016/j.bmcl.2012.11.011
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triphenylphosphine; 1,1,1,3,3,3-hexachloro-propan-2-one / dichloromethane / 0.58 h / -10 - 20 °C
2: tetrakis(triphenylphosphine) palladium(0) / toluene / 1 h / Reflux
3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C
4: ethanol / 24 h / Reflux
5: palladium 10% on activated carbon; cyclohexa-1,4-diene / ethanol / 24 h / Reflux
With
tetrakis(triphenylphosphine) palladium(0); 1,1,1,3,3,3-hexachloro-propan-2-one; cyclohexa-1,4-diene; palladium 10% on activated carbon; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine;
In
ethanol; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2012.11.011
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C
2: ethanol / 24 h / Reflux
3: palladium 10% on activated carbon; cyclohexa-1,4-diene / ethanol / 24 h / Reflux
With
cyclohexa-1,4-diene; palladium 10% on activated carbon; 3-chloro-benzenecarboperoxoic acid;
In
ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2012.11.011