(S)-3-methyl-2-(2-nitrophenylsulfonamido)-N-((1R,2R)-2-(2-nitrophenylsulfonamido)cyclohexyl)-butanamide

Base Information

Chemical Name:(S)-3-methyl-2-(2-nitrophenylsulfonamido)-N-((1R,2R)-2-(2-nitrophenylsulfonamido)cyclohexyl)-butanamide
CAS No.:1350538-35-0
Molecular Formula:C₂₃H₂₉N₅O₉S₂
Molecular Weight:583.643
Hs Code.:

Synonyms:(S)-3-methyl-2-(2-nitrophenylsulfonamido)-N-((1R,2R)-2-(2-nitrophenylsulfonamido)cyclohexyl)-butanamide

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Chemical Property of (S)-3-methyl-2-(2-nitrophenylsulfonamido)-N-((1R,2R)-2-(2-nitrophenylsulfonamido)cyclohexyl)-butanamide

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Technology Process of (S)-3-methyl-2-(2-nitrophenylsulfonamido)-N-((1R,2R)-2-(2-nitrophenylsulfonamido)cyclohexyl)-butanamide

There total 6 articles about (S)-3-methyl-2-(2-nitrophenylsulfonamido)-N-((1R,2R)-2-(2-nitrophenylsulfonamido)cyclohexyl)-butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1350538-33-8
N-(2-aminocyclohexyl)-2-nitrobenzene-1-sulfonamide

: 199783-36-3
(S)-3-methyl-2-(2-nitrophenylsulfonamido)butanoic acid

: 1350538-35-0
(S)-3-methyl-2-(2-nitrophenylsulfonamido)-N-((1R,2R)-2-(2-nitrophenylsulfonamido)cyclohexyl)-butanamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; at 0 - 20 ℃; for 8h;
DOI:10.3987/COM-11-12249

Reference yield:

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 1350538-35-0
(S)-3-methyl-2-(2-nitrophenylsulfonamido)-N-((1R,2R)-2-(2-nitrophenylsulfonamido)cyclohexyl)-butanamide

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 3.5 h / 0 - 20 °C

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 8 h / 0 - 20 °C

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane;
DOI:10.3987/COM-11-12249

Reference yield:

: 32044-22-7,39961-95-0
trans-1,2-(R,R)-diammoniumcyclohexane tartrate

: 1350538-35-0
(S)-3-methyl-2-(2-nitrophenylsulfonamido)-N-((1R,2R)-2-(2-nitrophenylsulfonamido)cyclohexyl)-butanamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; sodium hydroxide / dichloromethane / 0.17 h / 0 °C

2: dichloromethane / 3.5 h / 0 - 20 °C

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 8 h / 0 - 20 °C

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane;
DOI:10.3987/COM-11-12249