5-[(6S,7S,8R)-8-(3,4-Dimethoxy-phenyl)-3-methoxy-6,7-bis-methoxymethyl-5,6,7,8-tetrahydro-naphthalen-1-yloxy]-1-phenyl-1H-tetrazole

Base Information

• Chemical Name: 5-[(6S,7S,8R)-8-(3,4-Dimethoxy-phenyl)-3-methoxy-6,7-bis-methoxymethyl-5,6,7,8-tetrahydro-naphthalen-1-yloxy]-1-phenyl-1H-tetrazole
• CAS No.: 610310-56-0
• Molecular Formula: C₃₀H₃₄N₄O₆
• Molecular Weight: 546.623

Synonyms:5-[(6S,7S,8R)-8-(3,4-Dimethoxy-phenyl)-3-methoxy-6,7-bis-methoxymethyl-5,6,7,8-tetrahydro-naphthalen-1-yloxy]-1-phenyl-1H-tetrazole

Chemical Property of 5-[(6S,7S,8R)-8-(3,4-Dimethoxy-phenyl)-3-methoxy-6,7-bis-methoxymethyl-5,6,7,8-tetrahydro-naphthalen-1-yloxy]-1-phenyl-1H-tetrazole

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Technology Process of 5-[(6S,7S,8R)-8-(3,4-Dimethoxy-phenyl)-3-methoxy-6,7-bis-methoxymethyl-5,6,7,8-tetrahydro-naphthalen-1-yloxy]-1-phenyl-1H-tetrazole

There total 1 articles about 5-[(6S,7S,8R)-8-(3,4-Dimethoxy-phenyl)-3-methoxy-6,7-bis-methoxymethyl-5,6,7,8-tetrahydro-naphthalen-1-yloxy]-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hypophyllanthin → 5-[(6S,7S,8R)-8-(3,4-Dimethoxy-phenyl)-3-methoxy-6,7-bis-methoxymethyl-5,6,7,8-tetrahydro-naphthalen-1-yloxy]-1-phenyl-1H-tetrazole (610310-56-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 66 percent / Na; liquid ammonia / tetrahydrofuran / 2 h / -70 °C

2: 82.1 percent / K₂CO₃ / tetrahydrofuran / Heating

With ammonia; sodium; potassium carbonate; In tetrahydrofuran;

DOI:10.1016/S0031-9422(03)00371-6

Reference yield: 48.0%

5-[(6S,7S,8R)-8-(3,4-Dimethoxy-phenyl)-3-methoxy-6,7-bis-methoxymethyl-5,6,7,8-tetrahydro-naphthalen-1-yloxy]-1-phenyl-1H-tetrazole (610310-56-0) → 4-demethoxyphyltetralin

Guidance literature:

With hydrogen; acetic acid; palladium on activated charcoal; for 96h; under 3878.61 Torr;

DOI:10.1016/S0031-9422(03)00371-6

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