1-O-<11-(Methoxycarbonyl)undecyl>-2-O-methyl-sn-3-glyceryl o-chlorophenyl (p-nitrophenyl)ethyl phosphate

Base Information

Chemical Name:1-O-<11-(Methoxycarbonyl)undecyl>-2-O-methyl-sn-3-glyceryl o-chlorophenyl (p-nitrophenyl)ethyl phosphate
CAS No.:153959-49-0
Molecular Formula:C₃₁H₄₅ClNO₁₀P
Molecular Weight:658.126
Hs Code.:

Synonyms:1-O-<11-(Methoxycarbonyl)undecyl>-2-O-methyl-sn-3-glyceryl o-chlorophenyl (p-nitrophenyl)ethyl phosphate

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Chemical Property of 1-O-<11-(Methoxycarbonyl)undecyl>-2-O-methyl-sn-3-glyceryl o-chlorophenyl (p-nitrophenyl)ethyl phosphate

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Technology Process of 1-O-<11-(Methoxycarbonyl)undecyl>-2-O-methyl-sn-3-glyceryl o-chlorophenyl (p-nitrophenyl)ethyl phosphate

There total 7 articles about 1-O-<11-(Methoxycarbonyl)undecyl>-2-O-methyl-sn-3-glyceryl o-chlorophenyl (p-nitrophenyl)ethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 505-95-3
12-hydroxydodecanoic acid

: 153959-49-0
1-O-<11-(Methoxycarbonyl)undecyl>-2-O-methyl-sn-3-glyceryl o-chlorophenyl (p-nitrophenyl)ethyl phosphate

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / 1 M HCl / 12 h / Ambient temperature

2: 71.7 percent / BF₃*Et₂O / CHCl₃ / Ambient temperature

3: NaH / hexane; tetrahydrofuran

4: TBAF / tetrahydrofuran

5: pyridine / tetrahydrofuran / 30 h / Ambient temperature

With pyridine; hydrogenchloride; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; hexane; chloroform;
DOI:10.1021/jo00082a009

Reference yield:

: 71655-36-2
methyl 12-hydroxydodecanoate

: 153959-49-0
1-O-<11-(Methoxycarbonyl)undecyl>-2-O-methyl-sn-3-glyceryl o-chlorophenyl (p-nitrophenyl)ethyl phosphate

Guidance literature:: Multi-step reaction with 4 steps

1: 71.7 percent / BF₃*Et₂O / CHCl₃ / Ambient temperature

2: NaH / hexane; tetrahydrofuran

3: TBAF / tetrahydrofuran

4: pyridine / tetrahydrofuran / 30 h / Ambient temperature

With pyridine; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; hexane; chloroform;
DOI:10.1021/jo00082a009

Reference yield:

: 100-27-6
2-(4-nitrophenyl)ethanol

: 153959-49-0
1-O-<11-(Methoxycarbonyl)undecyl>-2-O-methyl-sn-3-glyceryl o-chlorophenyl (p-nitrophenyl)ethyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / tetrahydrofuran / 2 h / Ambient temperature

2: pyridine / tetrahydrofuran / 30 h / Ambient temperature

With pyridine; In tetrahydrofuran;
DOI:10.1021/jo00082a009