7-(4-methoxybenzyloxy)-8-{[phenethyl-(4-methoxybenzyl)amino]methyl}-2-methylchromone

Base Information

Chemical Name:7-(4-methoxybenzyloxy)-8-{[phenethyl-(4-methoxybenzyl)amino]methyl}-2-methylchromone
CAS No.:912353-07-2
Molecular Formula:C₃₅H₃₅NO₅
Molecular Weight:549.667
Hs Code.:

Synonyms:7-(4-methoxybenzyloxy)-8-{[phenethyl-(4-methoxybenzyl)amino]methyl}-2-methylchromone

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Chemical Property of 7-(4-methoxybenzyloxy)-8-{[phenethyl-(4-methoxybenzyl)amino]methyl}-2-methylchromone

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Technology Process of 7-(4-methoxybenzyloxy)-8-{[phenethyl-(4-methoxybenzyl)amino]methyl}-2-methylchromone

There total 5 articles about 7-(4-methoxybenzyloxy)-8-{[phenethyl-(4-methoxybenzyl)amino]methyl}-2-methylchromone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 912353-08-3
7-(4-methoxybenzyloxy)-2-methyl-8-((phenethylamino)methyl)-4H-chromen-4-one

: 824-94-2
p-methoxybenzyl chloride

: 912353-07-2
7-(4-methoxybenzyloxy)-8-{[phenethyl-(4-methoxybenzyl)amino]methyl}-2-methylchromone

Guidance literature:: With sodium hydride; sodium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1016/j.ejmech.2006.04.008

Reference yield: 12.0%

: 912353-06-1
8-((4-methoxybenzylamino)methyl)-7-(4-methoxybenzyloxy)-2-methyl-4H-chromen-4-one

: 103-63-9
1-phenyl-2-bromoethane

: 912353-07-2
7-(4-methoxybenzyloxy)-8-{[phenethyl-(4-methoxybenzyl)amino]methyl}-2-methylchromone

Guidance literature:: With sodium hydride; sodium iodide; In N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2006.04.008

Reference yield:

: 912353-05-0
7-(4-methoxybenzyloxy)-2-methyl-8-formylchromone

: 912353-07-2
7-(4-methoxybenzyloxy)-8-{[phenethyl-(4-methoxybenzyl)amino]methyl}-2-methylchromone

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / NaBH₄ / methanol

2: 57 percent / NaH; NaI / dimethylformamide / 2 h / 20 °C

With sodium tetrahydroborate; sodium hydride; sodium iodide; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2006.04.008