C₄₇H₅₇N₇O₇

Base Information

Chemical Name:C₄₇H₅₇N₇O₇
CAS No.:1613056-54-4
Molecular Formula:C₄₇H₅₇N₇O₇
Molecular Weight:832.012
Hs Code.:

C<sub>47</sub>H<sub>57</sub>N<sub>7</sub>O<sub>7</sub>

Synonyms:C₄₇H₅₇N₇O₇

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Chemical Property of C₄₇H₅₇N₇O₇

Chemical Property:

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Technology Process of C₄₇H₅₇N₇O₇

There total 22 articles about C₄₇H₅₇N₇O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1612236-46-0
C₁₈H₂₄IN₃O₄

: 1613056-53-3
C₃₅H₄₅BN₄O₅

: 1613056-54-4
C₄₇H₅₇N₇O₇

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,2-dimethoxyethane; water; at 90 ℃; for 4h; Inert atmosphere; Sealed tube;

Reference yield:

: 1612236-53-9
C₁₂H₁₄O

: 1613056-54-4
C₄₇H₅₇N₇O₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-iodo-succinimide / tetrahydrofuran; acetonitrile / 0.17 h / Inert atmosphere; Sealed tube

1.2: 5 h / 20 °C / Inert atmosphere; Sealed tube

2.1: boron tribromide / dichloromethane / 4.16 h / -78 - 20 °C / Inert atmosphere; Sealed tube

3.1: pyridine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere; Sealed tube

3.2: 1 h / 0 - 20 °C / Inert atmosphere; Sealed tube

4.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dimethoxyethane / 5 h / 90 °C / Inert atmosphere; Sealed tube

5.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / N,N-dimethyl-formamide / 3 h / 90 °C / Inert atmosphere; Sealed tube

6.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dimethoxyethane / 4 h / 90 °C / Inert atmosphere; Sealed tube

With pyridine; N-iodo-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; boron tribromide; potassium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1612236-54-0
C₁₂H₁₃IO

: 1613056-54-4
C₄₇H₅₇N₇O₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: boron tribromide / dichloromethane / 4.16 h / -78 - 20 °C / Inert atmosphere; Sealed tube

2.1: pyridine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere; Sealed tube

2.2: 1 h / 0 - 20 °C / Inert atmosphere; Sealed tube

3.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dimethoxyethane / 5 h / 90 °C / Inert atmosphere; Sealed tube

4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / N,N-dimethyl-formamide / 3 h / 90 °C / Inert atmosphere; Sealed tube

5.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dimethoxyethane / 4 h / 90 °C / Inert atmosphere; Sealed tube

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; boron tribromide; potassium carbonate; In 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide;